N-[9-(4-Benzenesulfonylaminocarbonyl-2-methoxy-benzyl)-9H-carbazol-2-yl]-2-cyclopentyl-acetamide

Base Information

Chemical Name:N-[9-(4-Benzenesulfonylaminocarbonyl-2-methoxy-benzyl)-9H-carbazol-2-yl]-2-cyclopentyl-acetamide
CAS No.:142535-01-1
Molecular Formula:C₃₄H₃₃N₃O₅S
Molecular Weight:595.719
Hs Code.:

Synonyms:N-[9-(4-Benzenesulfonylaminocarbonyl-2-methoxy-benzyl)-9H-carbazol-2-yl]-2-cyclopentyl-acetamide

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Chemical Property of N-[9-(4-Benzenesulfonylaminocarbonyl-2-methoxy-benzyl)-9H-carbazol-2-yl]-2-cyclopentyl-acetamide

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Technology Process of N-[9-(4-Benzenesulfonylaminocarbonyl-2-methoxy-benzyl)-9H-carbazol-2-yl]-2-cyclopentyl-acetamide

There total 5 articles about N-[9-(4-Benzenesulfonylaminocarbonyl-2-methoxy-benzyl)-9H-carbazol-2-yl]-2-cyclopentyl-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 98-10-2
benzenesulfonamide

: 104447-28-1
4-[2-(2-Cyclopentyl-acetylamino)-carbazol-9-ylmethyl]-3-methoxy-benzoic acid

: 142535-01-1
N-[9-(4-Benzenesulfonylaminocarbonyl-2-methoxy-benzyl)-9H-carbazol-2-yl]-2-cyclopentyl-acetamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 8h; Ambient temperature;
DOI:10.1021/jm00091a010

Reference yield:

: 14191-22-1
2-nitrocarbazole

: 142535-01-1
N-[9-(4-Benzenesulfonylaminocarbonyl-2-methoxy-benzyl)-9H-carbazol-2-yl]-2-cyclopentyl-acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: K₂CO₃ / acetone

2: H₂ / Pd/C / ethyl acetate / 2585.7 Torr

3: 78 percent / Me₂N(CH₂)3N=C=NEt*HCl, DMAP / CH₂Cl₂

4: 65 percent / aq. LiOH / methanol; tetrahydrofuran / 6 h / Ambient temperature

5: 16 percent / 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride, 4-(dimethylamino)pyridine / CH₂Cl₂ / 8 h / Ambient temperature

With dmap; lithium hydroxide; hydrogen; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; acetone;
DOI:10.1021/jm00091a010

Reference yield:

: 70264-94-7
methyl 4-(bromomethyl)-3-methoxybenzoate

: 142535-01-1
N-[9-(4-Benzenesulfonylaminocarbonyl-2-methoxy-benzyl)-9H-carbazol-2-yl]-2-cyclopentyl-acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: K₂CO₃ / acetone

2: H₂ / Pd/C / ethyl acetate / 2585.7 Torr

3: 78 percent / Me₂N(CH₂)3N=C=NEt*HCl, DMAP / CH₂Cl₂

4: 65 percent / aq. LiOH / methanol; tetrahydrofuran / 6 h / Ambient temperature

5: 16 percent / 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride, 4-(dimethylamino)pyridine / CH₂Cl₂ / 8 h / Ambient temperature

With dmap; lithium hydroxide; hydrogen; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; acetone;
DOI:10.1021/jm00091a010