trans-{4-[(1S,2S)-1,2-dihydroxy-2-(6-methoxy-[1,5]naphthyridin-4-yl)-ethyl]-cyclohexyl}-carbamic acid tert-butyl ester

Base Information

Chemical Name:trans-{4-[(1S,2S)-1,2-dihydroxy-2-(6-methoxy-[1,5]naphthyridin-4-yl)-ethyl]-cyclohexyl}-carbamic acid tert-butyl ester
CAS No.:947142-07-6
Molecular Formula:C₂₂H₃₁N₃O₅
Molecular Weight:417.505
Hs Code.:

Synonyms:trans-{4-[(1S,2S)-1,2-dihydroxy-2-(6-methoxy-[1,5]naphthyridin-4-yl)-ethyl]-cyclohexyl}-carbamic acid tert-butyl ester

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Chemical Property of trans-{4-[(1S,2S)-1,2-dihydroxy-2-(6-methoxy-[1,5]naphthyridin-4-yl)-ethyl]-cyclohexyl}-carbamic acid tert-butyl ester

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Technology Process of trans-{4-[(1S,2S)-1,2-dihydroxy-2-(6-methoxy-[1,5]naphthyridin-4-yl)-ethyl]-cyclohexyl}-carbamic acid tert-butyl ester

There total 3 articles about trans-{4-[(1S,2S)-1,2-dihydroxy-2-(6-methoxy-[1,5]naphthyridin-4-yl)-ethyl]-cyclohexyl}-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: trans-{4-[(E)-2-(6-methoxy-[1,5]naphthyridin-4-yl)-vinyl]-cyclohexyl}-carbamic acid tert-butyl ester

: 947142-07-6
trans-{4-[(1S,2S)-1,2-dihydroxy-2-(6-methoxy-[1,5]naphthyridin-4-yl)-ethyl]-cyclohexyl}-carbamic acid tert-butyl ester

Guidance literature:: With potassium osmate(VI); 1,4-bis(dihydroquinine)phthalazine; methanesulfonamide; water; potassium carbonate; potassium hexacyanoferrate(III); In ethyl acetate; tert-butyl alcohol; at 20 ℃; for 11h;

Reference yield: 68.0%

: 947141-87-9
trans-{4-[(E)-2-(6-methoxy-[1,5]naphthyridin-4-yl)-vinyl]-cyclohexyl}-carbamic acid tert-butyl ester

: 947142-07-6
trans-{4-[(1S,2S)-1,2-dihydroxy-2-(6-methoxy-[1,5]naphthyridin-4-yl)-ethyl]-cyclohexyl}-carbamic acid tert-butyl ester

Guidance literature:: With methanesulfonamide; AD-mix-α; In water; tert-butyl alcohol; at 20 ℃;

Reference yield: 68.0%

: 3144-09-0
methanesulfonamide

: 947141-87-9
trans-{4-[(E)-2-(6-methoxy-[1,5]naphthyridin-4-yl)-vinyl]-cyclohexyl}-carbamic acid tert-butyl ester

: 947142-07-6
trans-{4-[(1S,2S)-1,2-dihydroxy-2-(6-methoxy-[1,5]naphthyridin-4-yl)-ethyl]-cyclohexyl}-carbamic acid tert-butyl ester

Guidance literature:: methanesulfonamide; trans-{4-[(E)-2-(6-methoxy-[1,5]naphthyridin-4-yl)-vinyl]-cyclohexyl}-carbamic acid tert-butyl ester; With AD-mix-α; In water; tert-butyl alcohol; at 20 ℃;

With sodium hydrogensulfite; In water; tert-butyl alcohol;