2-{Ethoxycarbonyl-[(4-nitro-phenyl)-hydrazono]-methyl}-isoquinolinium; bromide

Base Information

Chemical Name:2-{Ethoxycarbonyl-[(4-nitro-phenyl)-hydrazono]-methyl}-isoquinolinium; bromide
CAS No.:86380-97-4
Molecular Formula:Br*C₁₉H₁₇N₄O₄
Molecular Weight:445.272
Hs Code.:

Synonyms:2-{Ethoxycarbonyl-[(4-nitro-phenyl)-hydrazono]-methyl}-isoquinolinium; bromide

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Chemical Property of 2-{Ethoxycarbonyl-[(4-nitro-phenyl)-hydrazono]-methyl}-isoquinolinium; bromide

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Technology Process of 2-{Ethoxycarbonyl-[(4-nitro-phenyl)-hydrazono]-methyl}-isoquinolinium; bromide

There total 2 articles about 2-{Ethoxycarbonyl-[(4-nitro-phenyl)-hydrazono]-methyl}-isoquinolinium; bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 119-65-3
isoquinoline

: 20147-56-2
C₁₀H₁₀N₂O₂BrNO₂

: 86380-97-4
2-{Ethoxycarbonyl-[(4-nitro-phenyl)-hydrazono]-methyl}-isoquinolinium; bromide

Guidance literature:: In ethanol; at 30 - 40 ℃;
DOI:10.1016/S0040-4020(01)97638-0

Reference yield:

: 18795-00-1,77083-78-4,77083-80-8
ethyl 2-((4-nitrophenyl)hydrazono)-3-oxobutanoate

: 86380-97-4
2-{Ethoxycarbonyl-[(4-nitro-phenyl)-hydrazono]-methyl}-isoquinolinium; bromide

Guidance literature:: Multi-step reaction with 2 steps

1: Br₂, Sodium acetate / acetic acid; acetic anhydride / 0 - 5 °C

2: 70 percent / ethanol / 30 - 40 °C

With bromine; sodium acetate; In ethanol; acetic anhydride; acetic acid;
DOI:10.1016/S0040-4020(01)97638-0