Ethyl 2,6-dimethyl-10-(4'-methyl-3'-cyclohexenyl)-undeca-2E,6E,9E-trienoate

Base Information

Chemical Name:Ethyl 2,6-dimethyl-10-(4'-methyl-3'-cyclohexenyl)-undeca-2E,6E,9E-trienoate
CAS No.:83912-02-1
Molecular Formula:C₂₂H₃₄O₂
Molecular Weight:330.511
Hs Code.:

Synonyms:Ethyl 2,6-dimethyl-10-(4'-methyl-3'-cyclohexenyl)-undeca-2E,6E,9E-trienoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl 2,6-dimethyl-10-(4'-methyl-3'-cyclohexenyl)-undeca-2E,6E,9E-trienoate

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Technology Process of Ethyl 2,6-dimethyl-10-(4'-methyl-3'-cyclohexenyl)-undeca-2E,6E,9E-trienoate

There total 1 articles about Ethyl 2,6-dimethyl-10-(4'-methyl-3'-cyclohexenyl)-undeca-2E,6E,9E-trienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 3699-66-9
ethyl 2-diethoxyphosphorylpropionate

: 83912-01-0
4-Methyl-8-(4'-methyl-3-cyclohexenyl)-nona-4E,7E-dien-1-al

: 83912-02-1
Ethyl 2,6-dimethyl-10-(4'-methyl-3'-cyclohexenyl)-undeca-2E,6E,9E-trienoate

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 10 ℃; for 2h;

Reference yield: 63.0%

: 83912-02-1
Ethyl 2,6-dimethyl-10-(4'-methyl-3'-cyclohexenyl)-undeca-2E,6E,9E-trienoate

: 72154-87-1,83945-77-1
2,6-Dimethyl-10-(4'-methyl-3'-cyclohexenyl)-undeca-2E,6E,9E-trien-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In benzene; at 60 ℃; for 12h;

Reference yield:

: 83912-02-1
Ethyl 2,6-dimethyl-10-(4'-methyl-3'-cyclohexenyl)-undeca-2E,6E,9E-trienoate

: 72145-14-3,83945-78-2
2,6-Dimethyl-10-(4'-methyl-3'-cyclohexenyl)-undeca-2E,6E,9E-trienal

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / LiAlH₄ / benzene / 12 h / 60 °C

2: 57 percent / pyridinium chlorochromate, NaOAc / CH₂Cl₂ / 2.5 h / 10 °C

With lithium aluminium tetrahydride; sodium acetate; pyridinium chlorochromate; In dichloromethane; benzene;