2-(15-(4-((S)-3-(2-((S)-3-(biphenyl-4-yl)-2-hydroxypropoxy)ethoxy)-2-hydroxypropyl)-1H-1,2,3-triazol-1-yl)pentadecyl)-5,6-dimethoxy-3-methylcyclohexa-2,5-diene-1,4-dione

Base Information

Chemical Name:2-(15-(4-((S)-3-(2-((S)-3-(biphenyl-4-yl)-2-hydroxypropoxy)ethoxy)-2-hydroxypropyl)-1H-1,2,3-triazol-1-yl)pentadecyl)-5,6-dimethoxy-3-methylcyclohexa-2,5-diene-1,4-dione
CAS No.:1608464-12-5
Molecular Formula:C₄₆H₆₅N₃O₈
Molecular Weight:788.037
Hs Code.:

2-(15-(4-((S)-3-(2-((S)-3-(biphenyl-4-yl)-2-hydroxypropoxy)ethoxy)-2-hydroxypropyl)-1H-1,2,3-triazol-1-yl)pentadecyl)-5,6-dimethoxy-3-methylcyclohexa-2,5-diene-1,4-dione

Synonyms:2-(15-(4-((S)-3-(2-((S)-3-(biphenyl-4-yl)-2-hydroxypropoxy)ethoxy)-2-hydroxypropyl)-1H-1,2,3-triazol-1-yl)pentadecyl)-5,6-dimethoxy-3-methylcyclohexa-2,5-diene-1,4-dione

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Chemical Property of 2-(15-(4-((S)-3-(2-((S)-3-(biphenyl-4-yl)-2-hydroxypropoxy)ethoxy)-2-hydroxypropyl)-1H-1,2,3-triazol-1-yl)pentadecyl)-5,6-dimethoxy-3-methylcyclohexa-2,5-diene-1,4-dione

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Technology Process of 2-(15-(4-((S)-3-(2-((S)-3-(biphenyl-4-yl)-2-hydroxypropoxy)ethoxy)-2-hydroxypropyl)-1H-1,2,3-triazol-1-yl)pentadecyl)-5,6-dimethoxy-3-methylcyclohexa-2,5-diene-1,4-dione

There total 13 articles about 2-(15-(4-((S)-3-(2-((S)-3-(biphenyl-4-yl)-2-hydroxypropoxy)ethoxy)-2-hydroxypropyl)-1H-1,2,3-triazol-1-yl)pentadecyl)-5,6-dimethoxy-3-methylcyclohexa-2,5-diene-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₀H₇₃N₃O₁₀

: 1608464-12-5
2-(15-(4-((S)-3-(2-((S)-3-(biphenyl-4-yl)-2-hydroxypropoxy)ethoxy)-2-hydroxypropyl)-1H-1,2,3-triazol-1-yl)pentadecyl)-5,6-dimethoxy-3-methylcyclohexa-2,5-diene-1,4-dione

Guidance literature:: With pyridinium p-toluenesulfonate; In tert-butyl alcohol; for 24h; Reflux;
DOI:10.1016/j.ejmech.2014.03.062

Reference yield:

: 605-94-7
2,3-Dimethoxy-5-methyl-1,4-benzoquinone

: 1608464-12-5
2-(15-(4-((S)-3-(2-((S)-3-(biphenyl-4-yl)-2-hydroxypropoxy)ethoxy)-2-hydroxypropyl)-1H-1,2,3-triazol-1-yl)pentadecyl)-5,6-dimethoxy-3-methylcyclohexa-2,5-diene-1,4-dione

Guidance literature:: Multi-step reaction with 5 steps

1: ammonium persulfate; silver nitrate / water; acetonitrile / 5 h / 75 °C / Darkness

2: triethylamine; dmap / dichloromethane / 1 h / 23 °C

3: sodium bromide / acetone / 6.5 h / Reflux

4: sodium L-ascorbate; copper(ll) sulfate pentahydrate; sodium azide / N,N-dimethyl-formamide; water / 85 °C

5: pyridinium p-toluenesulfonate / tert-butyl alcohol / 24 h / Reflux

With dmap; ammonium persulfate; sodium azide; copper(ll) sulfate pentahydrate; pyridinium p-toluenesulfonate; silver nitrate; sodium L-ascorbate; triethylamine; sodium bromide; In dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.ejmech.2014.03.062

Reference yield:

: 764723-91-3
2-(15-hydroxypentadecyl)-3-methyl-5,6-dimethoxy-1,4-benzoquinone

: 1608464-12-5
2-(15-(4-((S)-3-(2-((S)-3-(biphenyl-4-yl)-2-hydroxypropoxy)ethoxy)-2-hydroxypropyl)-1H-1,2,3-triazol-1-yl)pentadecyl)-5,6-dimethoxy-3-methylcyclohexa-2,5-diene-1,4-dione

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; dmap / dichloromethane / 1 h / 23 °C

2: sodium bromide / acetone / 6.5 h / Reflux

3: sodium L-ascorbate; copper(ll) sulfate pentahydrate; sodium azide / N,N-dimethyl-formamide; water / 85 °C

4: pyridinium p-toluenesulfonate / tert-butyl alcohol / 24 h / Reflux

With dmap; sodium azide; copper(ll) sulfate pentahydrate; pyridinium p-toluenesulfonate; sodium L-ascorbate; triethylamine; sodium bromide; In dichloromethane; water; N,N-dimethyl-formamide; acetone; tert-butyl alcohol;
DOI:10.1016/j.ejmech.2014.03.062