methyl N-imidazo[1,2-d][1,2,4]thiadiazol-3-yl-N-(6-{[(2-nitrophenyl)-sulfonyl]amino}hexyl)glycinate

Base Information

Chemical Name:methyl N-imidazo[1,2-d][1,2,4]thiadiazol-3-yl-N-(6-{[(2-nitrophenyl)-sulfonyl]amino}hexyl)glycinate
CAS No.:606969-89-5
Molecular Formula:C₁₉H₂₄N₆O₆S₂
Molecular Weight:496.568
Hs Code.:

Synonyms:methyl N-imidazo[1,2-d][1,2,4]thiadiazol-3-yl-N-(6-{[(2-nitrophenyl)-sulfonyl]amino}hexyl)glycinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl N-imidazo[1,2-d][1,2,4]thiadiazol-3-yl-N-(6-{[(2-nitrophenyl)-sulfonyl]amino}hexyl)glycinate

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Technology Process of methyl N-imidazo[1,2-d][1,2,4]thiadiazol-3-yl-N-(6-{[(2-nitrophenyl)-sulfonyl]amino}hexyl)glycinate

There total 11 articles about methyl N-imidazo[1,2-d][1,2,4]thiadiazol-3-yl-N-(6-{[(2-nitrophenyl)-sulfonyl]amino}hexyl)glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.5%

: 606969-89-5
methyl N-imidazo[1,2-d][1,2,4]thiadiazol-3-yl-N-(6-{[(2-nitrophenyl)-sulfonyl]amino}hexyl)glycinate

Guidance literature:

Reference yield: 75.0%

: 606969-03-3
3-[(4-methylphenyl)sulfonyl]imidazo[1,2-d][1,2,4]thiadiazole

: 863983-38-4
[6-(2-nitrobenzenesulfonylamino)hexylamino]acetic acid methyl ester

: 606969-89-5
methyl N-imidazo[1,2-d][1,2,4]thiadiazol-3-yl-N-(6-{[(2-nitrophenyl)-sulfonyl]amino}hexyl)glycinate

Guidance literature:: In dimethyl sulfoxide; at 20 ℃; for 16h;
DOI:10.1021/jo0507486

Reference yield:

: 124-09-4
1,6-Hexanediamine

: 606969-89-5
methyl N-imidazo[1,2-d][1,2,4]thiadiazol-3-yl-N-(6-{[(2-nitrophenyl)-sulfonyl]amino}hexyl)glycinate

Guidance literature:: Multi-step reaction with 5 steps

1: 79 percent / CH₂Cl₂ / 20 °C

2: 60 percent / triethylamine / CH₂Cl₂ / 16 h / 20 °C

3: 49 percent / triethylamine / dimethylsulfoxide / 20 °C

4: 55 percent / trifluoroacetic acid / CH₂Cl₂ / 16 h / 20 °C

5: K₂CO₃ / acetone

With potassium carbonate; triethylamine; trifluoroacetic acid; In dichloromethane; dimethyl sulfoxide; acetone;
DOI:10.1021/jo0507486