Technology Process of C17H20O2
There total 9 articles about C17H20O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
diethyl ether;
at 0 ℃;
for 0.5h;
DOI:10.1021/ja066374v
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 72 percent / PCC; 4 Angstroem molecular sieves / CH2Cl2 / 4 h / 20 °C
2.1: diisopropylamine; n-butyllithium / tetrahydrofuran; petroleum ether / 0.5 h / -78 °C
2.2: tetrahydrofuran; petroleum ether / 0.05 h / -78 °C
3.1: 417 mg / LAH / diethyl ether / 0.5 h / 0 °C
4.1: K2CO3 / methanol / 3 h / 20 °C
5.1: triethylamine / CH2Cl2 / 3 h / 20 °C
6.1: NaH / various solvent(s); tetrahydrofuran / 0.17 h / 0 °C
6.2: tetrahydrofuran; various solvent(s) / 2 h
7.1: 31 mg / LAH / diethyl ether / 0.5 h / 0 °C
With
lithium aluminium tetrahydride; n-butyllithium; 4 A molecular sieve; sodium hydride; potassium carbonate; triethylamine; diisopropylamine; pyridinium chlorochromate;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; Petroleum ether;
DOI:10.1021/ja066374v
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 417 mg / LAH / diethyl ether / 0.5 h / 0 °C
2.1: K2CO3 / methanol / 3 h / 20 °C
3.1: triethylamine / CH2Cl2 / 3 h / 20 °C
4.1: NaH / various solvent(s); tetrahydrofuran / 0.17 h / 0 °C
4.2: tetrahydrofuran; various solvent(s) / 2 h
5.1: 31 mg / LAH / diethyl ether / 0.5 h / 0 °C
With
lithium aluminium tetrahydride; sodium hydride; potassium carbonate; triethylamine;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1021/ja066374v