(3aR,7S,7aS*)-N-benzyl-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole

Base Information

Chemical Name:(3aR*,7S*,7aS*)-N-benzyl-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole
CAS No.:82281-29-6
Molecular Formula:C₂₂H₂₃NO₂
Molecular Weight:333.43
Hs Code.:

Synonyms:(3aR*,7S*,7aS*)-N-benzyl-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole

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Chemical Property of (3aR*,7S*,7aS*)-N-benzyl-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole

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Technology Process of (3aR*,7S*,7aS*)-N-benzyl-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole

There total 7 articles about (3aR*,7S*,7aS*)-N-benzyl-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 82281-24-1,82281-25-2,82281-26-3
N-benzyl-2-oxo-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole

: 82281-28-5
(3aR*,7R*,7aR*)-N-benzyl-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole

: 82281-29-6
(3aR*,7S*,7aS*)-N-benzyl-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 2h; Ambient temperature;
DOI:10.1021/jo00140a008

Reference yield:

: 82281-23-0
(E)-N-benzyl-N-<<3,4-(methylenedioxy)benzylidene>methyl>-2-(2,5-dihydro-1,1-dioxothienyl)acetamide

: 82281-29-6
(3aR*,7S*,7aS*)-N-benzyl-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / toluene / 2 h / Heating

2: 45 percent / xylene / 18 h / Heating

3: 51 percent / LiAlH₄ / diethyl ether / 2 h / Ambient temperature

With lithium aluminium tetrahydride; In diethyl ether; toluene; xylene;
DOI:10.1021/jo00140a008

Reference yield:

: 620601-36-7
[2-Benzo[1,3]dioxol-5-yl-eth-(Z)-ylidene]-benzyl-amine

: 82281-29-6
(3aR*,7S*,7aS*)-N-benzyl-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole

Guidance literature:: Multi-step reaction with 4 steps

1: N,N-diethylaniline / benzene / 1.) -78 deg C, 2 h, 2.) RT, 2 h

2: 97 percent / toluene / 2 h / Heating

3: 45 percent / xylene / 18 h / Heating

4: 51 percent / LiAlH₄ / diethyl ether / 2 h / Ambient temperature

With lithium aluminium tetrahydride; N,N-diethylaniline; In diethyl ether; toluene; xylene; benzene;
DOI:10.1021/jo00140a008