methyl 4-[(2S)-2-(N-benzyl-N-((2S)-2-hydroxy-3-phenoxypropyl)amino]-3-hydroxypropyl]benzoate

Base Information

• Chemical Name: methyl 4-[(2S)-2-(N-benzyl-N-((2S)-2-hydroxy-3-phenoxypropyl)amino]-3-hydroxypropyl]benzoate
• CAS No.: 357408-93-6
• Molecular Formula: C₂₇H₃₁NO₅
• Molecular Weight: 449.547

Synonyms:methyl 4-[(2S)-2-(N-benzyl-N-((2S)-2-hydroxy-3-phenoxypropyl)amino]-3-hydroxypropyl]benzoate

Chemical Property of methyl 4-[(2S)-2-(N-benzyl-N-((2S)-2-hydroxy-3-phenoxypropyl)amino]-3-hydroxypropyl]benzoate

Chemical Property:

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Technology Process of methyl 4-[(2S)-2-(N-benzyl-N-((2S)-2-hydroxy-3-phenoxypropyl)amino]-3-hydroxypropyl]benzoate

There total 1 articles about methyl 4-[(2S)-2-(N-benzyl-N-((2S)-2-hydroxy-3-phenoxypropyl)amino]-3-hydroxypropyl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrakis(triphenylphosphine) palladium(0) (14221-01-3) + 4-[(2S)-2-[N-benzyl-N-((2S)-2-hydroxy-3-phenoxypropyl)amino]-3-hydroxypropyl]phenyl trifluoro-methanesulfonate (357408-92-5) + 1,3-bis-(diphenylphosphino)propane (6737-42-4) → methyl 4-[(2S)-2-(N-benzyl-N-((2S)-2-hydroxy-3-phenoxypropyl)amino]-3-hydroxypropyl]benzoate (357408-93-6)

Guidance literature:

With triethylamine; carbon monoxide; In methanol; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

methyl 4-[(2S)-2-(N-benzyl-N-((2S)-2-hydroxy-3-phenoxypropyl)amino]-3-hydroxypropyl]benzoate (357408-93-6) → (2S)-3-[4-(hydroxymethyl)phenyl]-2-[((2S)-2-hydroxy-3-phenoxypropyl)amino]-1-propanol (357408-94-7)

Guidance literature:

palladium on activated carbon; hydrogen; In tetrahydrofuran; hydrogenchloride; methanol; water; ethyl acetate;

Reference yield:

methyl 4-[(2S)-2-(N-benzyl-N-((2S)-2-hydroxy-3-phenoxypropyl)amino]-3-hydroxypropyl]benzoate (357408-93-6) → 4-[(2S)-3-hydroxy-2-[((2S)-2-hydroxy-3-phenoxypropyl)amino]propyl]-benzoic acid (357408-95-8)

Guidance literature:

palladium on activated carbon; hydrogen; In tetrahydrofuran; methanol; sodium hydroxide; ethyl acetate;

upstream raw materials:

tetrakis(triphenylphosphine) palladium⁽⁰⁾

4-[(2S)-2-[N-benzyl-N-((2S)-2-hydroxy-3-phenoxypropyl)amino]-3-hydroxypropyl]phenyl trifluoro-methanesulfonate

1,3-bis-(diphenylphosphino)propane

Downstream raw materials:

(2S)-3-[4-(hydroxymethyl)phenyl]-2-[((2S)-2-hydroxy-3-phenoxypropyl)amino]-1-propanol

4-[(2S)-3-hydroxy-2-[((2S)-2-hydroxy-3-phenoxypropyl)amino]propyl]-benzoic acid

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