11-(4-chlorophenyl)-3,3-dimethyl-11-3,4-dihydro-1H-pyridazino[1,2-a]indazole-1,6,9(2H,11H)-trione

Base Information

Chemical Name:11-(4-chlorophenyl)-3,3-dimethyl-11-3,4-dihydro-1H-pyridazino[1,2-a]indazole-1,6,9(2H,11H)-trione
CAS No.:1091592-75-4
Molecular Formula:C₁₉H₁₇ClN₂O₃
Molecular Weight:356.809
Hs Code.:

Synonyms:11-(4-chlorophenyl)-3,3-dimethyl-11-3,4-dihydro-1H-pyridazino[1,2-a]indazole-1,6,9(2H,11H)-trione

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Chemical Property of 11-(4-chlorophenyl)-3,3-dimethyl-11-3,4-dihydro-1H-pyridazino[1,2-a]indazole-1,6,9(2H,11H)-trione

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Technology Process of 11-(4-chlorophenyl)-3,3-dimethyl-11-3,4-dihydro-1H-pyridazino[1,2-a]indazole-1,6,9(2H,11H)-trione

There total 2 articles about 11-(4-chlorophenyl)-3,3-dimethyl-11-3,4-dihydro-1H-pyridazino[1,2-a]indazole-1,6,9(2H,11H)-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 123-33-1
Maleic hydrazide

: 104-88-1
4-chlorobenzaldehyde

: 126-81-8
dimedone

: 1091592-75-4
11-(4-chlorophenyl)-3,3-dimethyl-11-3,4-dihydro-1H-pyridazino[1,2-a]indazole-1,6,9(2H,11H)-trione

Guidance literature:: With 1-methyl-2-pyrrolidinone hydrosulfate; In neat (no solvent); at 85 ℃; for 0.0833333h; Green chemistry;
DOI:10.1002/jhet.1736

Reference yield: 73.0%

: 104-88-1
4-chlorobenzaldehyde

: 126-81-8
dimedone

: 123-33-1
3,6-dihydroxypyridazine

: 1091592-75-4
11-(4-chlorophenyl)-3,3-dimethyl-11-3,4-dihydro-1H-pyridazino[1,2-a]indazole-1,6,9(2H,11H)-trione

Guidance literature:: With toluene-4-sulfonic acid; at 70 ℃; for 0.166667h; capped vial; neat (no solvent);
DOI:10.3184/030823409X12506792542701