C₄₀H₁₆F₁₂O₂

Base Information

• Chemical Name: C₄₀H₁₆F₁₂O₂
• CAS No.: 1380099-45-5
• Molecular Formula: C₄₀H₁₆F₁₂O₂
• Molecular Weight: 756.547
• Mol file: 1380099-45-5.mol

Synonyms:C₄₀H₁₆F₁₂O₂

Chemical Property of C₄₀H₁₆F₁₂O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₀H₁₆F₁₂O₂

There total 4 articles about C₄₀H₁₆F₁₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2'-(2,6-dimethylnaphthalene-1,5-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane) (1228673-46-8) → C40H16F12O2 (1380099-45-5)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 665 h / 78 °C / Inert atmosphere

2: water; potassium permanganate / pyridine / 95 °C

3: sulfuric acid / water / 3 h / 85 °C

4: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 8 h / Inert atmosphere; Reflux

With potassium permanganate; sulfuric acid; water; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In pyridine; 1,2-dimethoxyethane; water; toluene;

Reference yield:

C24H18Br2 (1228673-47-9) → C40H16F12O2 (1380099-45-5)

Guidance literature:

Multi-step reaction with 3 steps

1: water; potassium permanganate / pyridine / 95 °C

2: sulfuric acid / water / 3 h / 85 °C

3: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 8 h / Inert atmosphere; Reflux

With potassium permanganate; sulfuric acid; water; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In pyridine; water; toluene;

Reference yield:

1,5-Dibromo-2,6-dimethylnaphthalene (20027-95-6) → C40H16F12O2 (1380099-45-5)

Guidance literature:

Multi-step reaction with 5 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 65 h / 80 °C

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 665 h / 78 °C / Inert atmosphere

3: water; potassium permanganate / pyridine / 95 °C

4: sulfuric acid / water / 3 h / 85 °C

5: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 8 h / Inert atmosphere; Reflux

With potassium permanganate; sulfuric acid; water; sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In pyridine; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; toluene;

upstream raw materials:

1,5-Dibromo-2,6-dimethylnaphthalene

2,2'-(2,6-dimethylnaphthalene-1,5-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

C₂₄H₁₈Br₂

C₂₄H₁₄Br₂O₄

Downstream raw materials:

C₄₆H₁₆F₁₂N₄