2-amino-N-[4-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)butyl]benzamide

Base Information

Chemical Name:2-amino-N-[4-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)butyl]benzamide
CAS No.:916993-93-6
Molecular Formula:C₂₂H₂₉N₃O₃
Molecular Weight:383.491
Hs Code.:

Synonyms:2-amino-N-[4-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)butyl]benzamide

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Chemical Property of 2-amino-N-[4-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)butyl]benzamide

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Technology Process of 2-amino-N-[4-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)butyl]benzamide

There total 4 articles about 2-amino-N-[4-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)butyl]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 2-nitro-N-[4-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)butyl]benzamide

: 916993-93-6
2-amino-N-[4-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)butyl]benzamide

Guidance literature:: With ammonium chloride; zinc; In methanol; for 1.5h; Heating;
DOI:10.1016/j.bmc.2006.07.055

Reference yield:

: 1745-07-9
6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

: 916993-93-6
2-amino-N-[4-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)butyl]benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / sodium carbonate; sodium iodide / 2-methyl-propan-2-ol / 24 h / Heating

2: 99 percent / NaOH; hydrogen; nickel / ethanol / 12 h / 2068.59 Torr

3: 32 percent / Dowex 1X₈ chloride resin / ethyl acetate / 20 °C

4: 72 percent / ammonium chloride; zinc / methanol / 1.5 h / Heating

With sodium hydroxide; Dowex 1X₈ chloride resin; ammonium chloride; hydrogen; nickel; sodium carbonate; sodium iodide; zinc; In methanol; ethanol; ethyl acetate; tert-butyl alcohol;
DOI:10.1016/j.bmc.2006.07.055

Reference yield:

: 669067-80-5
4-(6,7-dimethoxy-3,4-dihydroisoquinoline-2(1H)-yl)-butan-1-amine

: 916993-93-6
2-amino-N-[4-(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)butyl]benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 32 percent / Dowex 1X₈ chloride resin / ethyl acetate / 20 °C

2: 72 percent / ammonium chloride; zinc / methanol / 1.5 h / Heating

With Dowex 1X₈ chloride resin; ammonium chloride; zinc; In methanol; ethyl acetate;
DOI:10.1016/j.bmc.2006.07.055