N--O-<2,3,4,6-tetrabenzyl-β-D-glucuronyl> carbamate

Base Information

Chemical Name:N--O-<2,3,4,6-tetrabenzyl-β-D-glucuronyl> carbamate
CAS No.:168072-93-3
Molecular Formula:C₄₄H₄₉NO₁₀
Molecular Weight:751.874
Hs Code.:

N-<allyl 3,3-dimethylbutanoate>-O-<2,3,4,6-tetrabenzyl-β-D-glucuronyl> carbamate

Synonyms:N--O-<2,3,4,6-tetrabenzyl-β-D-glucuronyl> carbamate

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Chemical Property of N--O-<2,3,4,6-tetrabenzyl-β-D-glucuronyl> carbamate

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Technology Process of N--O-<2,3,4,6-tetrabenzyl-β-D-glucuronyl> carbamate

There total 4 articles about N--O-<2,3,4,6-tetrabenzyl-β-D-glucuronyl> carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 4539-78-0
2,3,4-tri-O-benzyl-D-glucopyranosideuronic acid benzyl ester

: 168072-83-1
4-Isocyanato-3,3-dimethyl-butyric acid allyl ester

: 168072-93-3
N--O-<2,3,4,6-tetrabenzyl-β-D-glucuronyl> carbamate

Guidance literature:: With triethylamine; In toluene; a) 70 deg C, 24 h, b) reflux, 16 h;
DOI:10.1016/S0968-0896(96)00249-0

Reference yield:

: 4160-82-1
3,3-dimethylglutaric anhydride

: 168072-93-3
N--O-<2,3,4,6-tetrabenzyl-β-D-glucuronyl> carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / Et₃N, DMAP / 3 h

2: diphenylphosphorylazide, Et₃N / CH₂Cl₂ / 4 h

3: 130 °C / 1 Torr

4: 87 percent / Et₃N / toluene / a) 70 deg C, 24 h, b) reflux, 16 h

With dmap; diphenylphosphoranyl azide; triethylamine; In dichloromethane; toluene;
DOI:10.1016/S0968-0896(96)00249-0

Reference yield:

: 168072-78-4
1-allyl-3,3-dimethylglutaric ester

: 168072-93-3
N--O-<2,3,4,6-tetrabenzyl-β-D-glucuronyl> carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: diphenylphosphorylazide, Et₃N / CH₂Cl₂ / 4 h

2: 130 °C / 1 Torr

3: 87 percent / Et₃N / toluene / a) 70 deg C, 24 h, b) reflux, 16 h

With diphenylphosphoranyl azide; triethylamine; In dichloromethane; toluene;
DOI:10.1016/S0968-0896(96)00249-0