Fmoc-homotyrosine 4'-allyloxyphenylmethyl ether trimethylsilylethyl ester

Base Information

Chemical Name:Fmoc-homotyrosine 4'-allyloxyphenylmethyl ether trimethylsilylethyl ester
CAS No.:296774-47-5
Molecular Formula:C₄₀H₄₅NO₆Si
Molecular Weight:663.886
Hs Code.:

Synonyms:Fmoc-homotyrosine 4'-allyloxyphenylmethyl ether trimethylsilylethyl ester

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Chemical Property of Fmoc-homotyrosine 4'-allyloxyphenylmethyl ether trimethylsilylethyl ester

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Technology Process of Fmoc-homotyrosine 4'-allyloxyphenylmethyl ether trimethylsilylethyl ester

There total 3 articles about Fmoc-homotyrosine 4'-allyloxyphenylmethyl ether trimethylsilylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 3256-45-9
4-allyloxybenzyl alcohol

: Fmoc-homotyrosine trimethylsilylethyl ester

: 296774-47-5
Fmoc-homotyrosine 4'-allyloxyphenylmethyl ether trimethylsilylethyl ester

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 25 ℃;
DOI:10.1016/S0968-0896(00)00097-3

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 296774-47-5
Fmoc-homotyrosine 4'-allyloxyphenylmethyl ether trimethylsilylethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / EDAC; DMAP / CH₂Cl₂ / 5 h / 25 °C

2: 75 percent / Ph₃P; diethyl azodicarboxylate / tetrahydrofuran / 25 °C

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; 1: Esterification / 2: Etherification;
DOI:10.1016/S0968-0896(00)00097-3

Reference yield:

: 198560-10-0
Fmoc-hTyrOH

: 296774-47-5
Fmoc-homotyrosine 4'-allyloxyphenylmethyl ether trimethylsilylethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / EDAC; DMAP / CH₂Cl₂ / 5 h / 25 °C

2: 75 percent / Ph₃P; diethyl azodicarboxylate / tetrahydrofuran / 25 °C

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; 1: Esterification / 2: Etherification;
DOI:10.1016/S0968-0896(00)00097-3