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C28H45NO4Si

Base Information
  • Chemical Name:C28H45NO4Si
  • CAS No.:1345706-70-8
  • Molecular Formula:C28H45NO4Si
  • Molecular Weight:487.755
  • Hs Code.:
C<sub>28</sub>H<sub>45</sub>NO<sub>4</sub>Si

Synonyms:C28H45NO4Si

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Chemical Property of C28H45NO4Si
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Technology Process of C28H45NO4Si

There total 1 articles about C28H45NO4Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃;
DOI:10.1016/j.bmcl.2011.06.109
Guidance literature:
Multi-step reaction with 10 steps
1: lithium borohydride / tetrahydrofuran; methanol / 0 - 20 °C
2: Dess-Martin periodane / dichloromethane
3: sodium dihydrogenphosphate; sodium chlorite; 2-Methyl-1-butene / water; tert-butyl alcohol
4: 4-methyl-morpholine; HATU / N,N-dimethyl-formamide
5: ozone / methanol
6: triethylsilane; trifluoroacetic acid / dichloromethane / 0 °C
7: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C
8: lithium hydroxide / tetrahydrofuran / 20 °C
9: 4-methyl-morpholine; HATU / N,N-dimethyl-formamide
10: hydrogenchloride / 1,4-dioxane; water
With 4-methyl-morpholine; hydrogenchloride; triethylsilane; sodium chlorite; sodium dihydrogenphosphate; lithium borohydride; HATU; tetrabutyl ammonium fluoride; Dess-Martin periodane; ozone; 2-Methyl-1-butene; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2011.06.109
Guidance literature:
Multi-step reaction with 4 steps
1: lithium borohydride / tetrahydrofuran; methanol / 0 - 20 °C
2: Dess-Martin periodane / dichloromethane
3: sodium dihydrogenphosphate; sodium chlorite; 2-Methyl-1-butene / water; tert-butyl alcohol
4: 4-methyl-morpholine; HATU / N,N-dimethyl-formamide
With 4-methyl-morpholine; sodium chlorite; sodium dihydrogenphosphate; lithium borohydride; HATU; Dess-Martin periodane; 2-Methyl-1-butene; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2011.06.109
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