Technology Process of C28H45NO4Si
There total 1 articles about C28H45NO4Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: lithium borohydride / tetrahydrofuran; methanol / 0 - 20 °C
2: Dess-Martin periodane / dichloromethane
3: sodium dihydrogenphosphate; sodium chlorite; 2-Methyl-1-butene / water; tert-butyl alcohol
4: 4-methyl-morpholine; HATU / N,N-dimethyl-formamide
5: ozone / methanol
6: triethylsilane; trifluoroacetic acid / dichloromethane / 0 °C
7: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C
8: lithium hydroxide / tetrahydrofuran / 20 °C
9: 4-methyl-morpholine; HATU / N,N-dimethyl-formamide
10: hydrogenchloride / 1,4-dioxane; water
With
4-methyl-morpholine; hydrogenchloride; triethylsilane; sodium chlorite; sodium dihydrogenphosphate; lithium borohydride; HATU; tetrabutyl ammonium fluoride; Dess-Martin periodane; ozone; 2-Methyl-1-butene; trifluoroacetic acid; lithium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2011.06.109
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium borohydride / tetrahydrofuran; methanol / 0 - 20 °C
2: Dess-Martin periodane / dichloromethane
3: sodium dihydrogenphosphate; sodium chlorite; 2-Methyl-1-butene / water; tert-butyl alcohol
4: 4-methyl-morpholine; HATU / N,N-dimethyl-formamide
With
4-methyl-morpholine; sodium chlorite; sodium dihydrogenphosphate; lithium borohydride; HATU; Dess-Martin periodane; 2-Methyl-1-butene;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2011.06.109