10-(3-methylphenyl)-7,8-benzoquinoline

Base Information

Chemical Name:10-(3-methylphenyl)-7,8-benzoquinoline
CAS No.:1127212-97-8
Molecular Formula:C₂₀H₁₅N
Molecular Weight:269.346
Hs Code.:

Synonyms:10-(3-methylphenyl)-7,8-benzoquinoline

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Chemical Property of 10-(3-methylphenyl)-7,8-benzoquinoline

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Technology Process of 10-(3-methylphenyl)-7,8-benzoquinoline

There total 9 articles about 10-(3-methylphenyl)-7,8-benzoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 230-27-3
7,8-benzoquinoline

: N,N-(Boc)_2-3-methylbenzamide

: 1127212-97-8
10-(3-methylphenyl)-7,8-benzoquinoline

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; tributyl-amine; water; In toluene; at 150 ℃; for 15h; chemoselective reaction;
DOI:10.1021/acscatal.7b02540

Reference yield: 96.0%

: 230-27-3
7,8-benzoquinoline

: 625-95-6
3-Iodotoluene

: 1127212-97-8
10-(3-methylphenyl)-7,8-benzoquinoline

Guidance literature:: With C₁₇H₂₁N₃NiO₃; lithium hexamethyldisilazane; In neat (no solvent); at 120 ℃; for 1h; Sealed tube; Glovebox; Green chemistry;
DOI:10.1002/cssc.201700321

Reference yield: 93.0%

: 230-27-3
7,8-benzoquinoline

: 28987-79-3
m-tolylmagnesium bromide

: 1127212-97-8
10-(3-methylphenyl)-7,8-benzoquinoline

Guidance literature:: With 2,3-dichlorobutane; N,N,N,N,-tetramethylethylenediamine; cobalt(III) acetylacetonate; In tetrahydrofuran; at 20 ℃; for 48h; regioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201005394