<(4-methylphenyl)sulfonyl>oxime of 1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one

Base Information

Chemical Name:<(4-methylphenyl)sulfonyl>oxime of 1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one
CAS No.:84131-95-3
Molecular Formula:C₂₅H₂₂N₂O₄S
Molecular Weight:446.527
Hs Code.:

<(4-methylphenyl)sulfonyl>oxime of 1-benzoyl-2,2a,3,4-tetrahydrobenz<cd>indol-5(1H)-one

Synonyms:<(4-methylphenyl)sulfonyl>oxime of 1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <(4-methylphenyl)sulfonyl>oxime of 1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one

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Technology Process of <(4-methylphenyl)sulfonyl>oxime of 1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one

There total 4 articles about <(4-methylphenyl)sulfonyl>oxime of 1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 84131-94-2
5-oxime of 1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one

: 98-59-9
p-toluenesulfonyl chloride

: 84131-95-3
<(4-methylphenyl)sulfonyl>oxime of 1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one

Guidance literature:: With pyridine; at 0 ℃;
DOI:10.1021/jm00358a012

Reference yield:

: 830-96-6
Indole-3-propionic acid

: 84131-95-3
<(4-methylphenyl)sulfonyl>oxime of 1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: Raney nickel; aqueous NaOH / 147102 - 220652 Torr / Hydrogenation_.Behandlung des Reaktionsprodukts mit Benzoylchlorid und wss. NaOH

2: thionyl chloride / Erwaermen des gebildeten Saeuerchlorids mit Aluminiumchlorid in Schwefelkohlenstoff

3: potassium carbonate; aqueous methanol; hydroxylamine hydrochloride

4: pyridine / 0 °C

With pyridine; methanol; sodium hydroxide; thionyl chloride; hydroxylamine hydrochloride; nickel; potassium carbonate;
DOI:10.1021/ja01594a039

Reference yield:

: 132008-45-8,51867-02-8
1-benzoyl-2,2a,3,4-tetrahydro-1H-benz[cd]indol-5-one

: 84131-95-3
<(4-methylphenyl)sulfonyl>oxime of 1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; aqueous methanol; hydroxylamine hydrochloride

2: pyridine / 0 °C

With pyridine; methanol; hydroxylamine hydrochloride; potassium carbonate;
DOI:10.1021/ja01594a039