(S)-2-(t-butoxycarbonylamino)-N-methyl-3-phenyl-N-(1,2-propadienyl)propanamide

Base Information

• Chemical Name: (S)-2-(t-butoxycarbonylamino)-N-methyl-3-phenyl-N-(1,2-propadienyl)propanamide
• CAS No.: 1133721-59-1
• Molecular Formula: C₁₈H₂₄N₂O₃
• Molecular Weight: 316.4

Synonyms:(S)-2-(t-butoxycarbonylamino)-N-methyl-3-phenyl-N-(1,2-propadienyl)propanamide

Chemical Property of (S)-2-(t-butoxycarbonylamino)-N-methyl-3-phenyl-N-(1,2-propadienyl)propanamide

Chemical Property:

Purity/Quality:

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Technology Process of (S)-2-(t-butoxycarbonylamino)-N-methyl-3-phenyl-N-(1,2-propadienyl)propanamide

There total 1 articles about (S)-2-(t-butoxycarbonylamino)-N-methyl-3-phenyl-N-(1,2-propadienyl)propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(S)-2-(t-butoxycarbonylamino)-N-methyl-3-phenyl-N-propargylpropanamide (1133721-54-6) → (S)-2-(t-butoxycarbonylamino)-N-methyl-3-phenyl-N-(1,2-propadienyl)propanamide (1133721-59-1)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 0.0166667h;

DOI:10.1016/j.tetlet.2009.01.074

Reference yield: 72.0%

(S)-2-(t-butoxycarbonylamino)-N-methyl-3-phenyl-N-(1,2-propadienyl)propanamide (1133721-59-1) → C18H24N2O3 (1140404-77-8)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at 50 ℃; for 0.5h; Microwave irradiation;

DOI:10.1016/j.tetlet.2009.01.074

Reference yield: 65.0%

(S)-2-(t-butoxycarbonylamino)-N-methyl-3-phenyl-N-(1,2-propadienyl)propanamide (1133721-59-1) → C18H24N2O3 (1175542-43-4)

Guidance literature:

With gold(III) chloride; In acetonitrile; for 1.5h; Inert atmosphere; Reflux;

DOI:10.1016/j.tetlet.2009.06.011

upstream raw materials:

(S)-2-(t-butoxycarbonylamino)-N-methyl-3-phenyl-N-propargylpropanamide

Downstream raw materials:

C₁₈H₂₄N₂O₃

C₁₈H₂₄N₂O₃

C₁₈H₂₄N₂O₃

(2S,5S)-5-benzyl-(t-butoxycarbonylamino)-3-methyl-2-(1-phenylvinyl)-2,3-dihydroimidazolidin-4(5H)-one

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