3,9,17,23-bis(ethane-1,1-p-phenol-2,2-p-phenoxy)phthalocyaninatozinc(II)

Base Information

• Chemical Name: 3,9,17,23-bis(ethane-1,1-p-phenol-2,2-p-phenoxy)phthalocyaninatozinc(II)
• CAS No.: 1265899-34-0
• Molecular Formula: C₈₄H₅₂N₈O₈Zn
• Molecular Weight: 1366.78

Synonyms:3,9,17,23-bis(ethane-1,1-p-phenol-2,2-p-phenoxy)phthalocyaninatozinc(II)

Chemical Property of 3,9,17,23-bis(ethane-1,1-p-phenol-2,2-p-phenoxy)phthalocyaninatozinc(II)

Chemical Property:

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Technology Process of 3,9,17,23-bis(ethane-1,1-p-phenol-2,2-p-phenoxy)phthalocyaninatozinc(II)

There total 2 articles about 3,9,17,23-bis(ethane-1,1-p-phenol-2,2-p-phenoxy)phthalocyaninatozinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.3%

4,4'-(ethane-1,1-p-phenol-2,2-p-phenoxy)phthalonitrile (1265899-33-9) → 3,9,17,23-bis(ethane-1,1-p-phenol-2,2-p-phenoxy)phthalocyaninatozinc(II) (1265899-34-0)

Guidance literature:

With zinc(II) acetate dihydrate; In pentan-1-ol; N,N-dimethyl-formamide; at 190 ℃; for 24h; Inert atmosphere;

DOI:10.1039/c0dt01163k

Reference yield: 74.3%

4,4'-(ethane-1,1-p-phenol-2,2-p-phenoxy)phthalonitrile (1265899-33-9) + zinc(II) acetate dihydrate (5970-45-6) → 3,9,17,23-bis(ethane-1,1-p-phenol-2,2-p-phenoxy)phthalocyaninatozinc(II) (1265899-34-0)

Guidance literature:

In N,N-dimethyl-formamide; (under Ar); mixt. of ligand and Zn(CH3CO2)2*2H2O in DMF refluxed for 24 h, cooled to room temp., treated with H2O; filtered, washed with common organic solvents; elem. anal.;

DOI:10.1039/c0dt01163k

Reference yield: 70.0%

3,9,17,23-bis(ethane-1,1-p-phenol-2,2-p-phenoxy)phthalocyaninatozinc(II) (1265899-34-0) → 3,9,17,23-bis(ethane-1,1-p-phenol-2,2-p-phenoxy)phthalo-cyaninatozinc(II) tetrapotassium

Guidance literature:

With potassium hydroxide; In water; for 0.166667h; Heating;

DOI:10.1039/c0dt01163k

upstream raw materials:

4,4'-(ethane-1,1-p-phenol-2,2-p-phenoxy)phthalonitrile

zinc(II) acetate dihydrate

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