S₄N₄

Base Information

• Chemical Name: S₄N₄
• CAS No.: 147730-18-5
• Molecular Formula: N₄S₄
• Molecular Weight: 184.291

Synonyms:S₄N₄

Chemical Property of S₄N₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of S₄N₄

There total 1 articles about S₄N₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thiotrithiazyl chloride (857244-78-1) → sulfur (10544-50-0) + S4N4 (147730-18-5) + thionitrosyl chloride (63788-84-1) + S3N2(1+)*Cl(1-)

Guidance literature:

With iron; In gas; on the surface if iron wire, 300°C, 11 h; trapped on KBr disc at -196°C, identified by i.r. spect. and elem. anal.;

DOI:10.1039/DT9800000731

Reference yield: 70.0%

ethylenebis(triphenylphosphine)platinum(0) (12120-15-9) + S4N4 (147730-18-5) → (P(C6H5)3)Pt(S2N2)2Pt(P(C6H5)3)*C6H6

Guidance literature:

With benzene; In benzene; a soln. of S4N4 in benzene was added under N2 to a soln. of (PPh3)2Pt(C2H4) in benzene at room temp.; crystals were filtered off, washed with CH2Cl2, light petroleum, dried;elem. anal., the presence of benzene solvate was shown by mass spectrum;

DOI:10.1016/0022-328X(85)80055-3

Reference yield: 50.0%

ethylenebis(triphenylphosphine)platinum(0) (12120-15-9) + S4N4 (147730-18-5) → [Pt2(S2N2)2(P(C6H5)3)2]

Guidance literature:

In tetrahydrofuran; benzene; a soln. of S4N4 in benzene was added under N2 to a soln. of (PPh3)2Pt(C2H4) in THF (benzene to THF ratio 2:1 v/v) at room temp.; sepd. crystals were collected, washed with CH2Cl2, benzene, light petroleum, dried; elem. anal.;

DOI:10.1016/0022-328X(85)80055-3

upstream raw materials:

thiotrithiazyl chloride

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