(all-rac)-acetic acid 4-hydroxy-2,3,6-trimethyl-5-[3-(4,8,12-trimethyltridecyl)-but-3-enyl]phenyl ester

Base Information

• Chemical Name: (all-rac)-acetic acid 4-hydroxy-2,3,6-trimethyl-5-[3-(4,8,12-trimethyltridecyl)-but-3-enyl]phenyl ester
• CAS No.: 696597-97-4
• Molecular Formula: C₃₁H₅₂O₃
• Molecular Weight: 472.752

Synonyms:(all-rac)-acetic acid 4-hydroxy-2,3,6-trimethyl-5-[3-(4,8,12-trimethyltridecyl)-but-3-enyl]phenyl ester

Chemical Property of (all-rac)-acetic acid 4-hydroxy-2,3,6-trimethyl-5-[3-(4,8,12-trimethyltridecyl)-but-3-enyl]phenyl ester

Chemical Property:

Purity/Quality:

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Technology Process of (all-rac)-acetic acid 4-hydroxy-2,3,6-trimethyl-5-[3-(4,8,12-trimethyltridecyl)-but-3-enyl]phenyl ester

There total 1 articles about (all-rac)-acetic acid 4-hydroxy-2,3,6-trimethyl-5-[3-(4,8,12-trimethyltridecyl)-but-3-enyl]phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

isophytol (505-32-8) + 4-acetoxy-2,3,5-trimethylphenol (36592-62-8) → 4-hydroxy-2,3,6-trimethyl-5-[(all-rac,Z)-3,7,11,15-tetramethylhexadec-2-en-1-yl]phenyl acetate + 4-hydroxy-2,3,6-trimethyl-5-[(all-rac,E)-3,7,11,15-tetramethylhexadec-2-en-1-yl]phenyl acetate + (all-rac)-acetic acid 4-hydroxy-2,3,6-trimethyl-5-[3-(4,8,12-trimethyltridecyl)-but-3-enyl]phenyl ester (696597-97-4) + vitamin E acetate (58-95-7,7695-91-2,18920-61-1,52225-20-4,54165-54-7,66900-46-7,79200-45-6,79200-46-7,79200-47-8,79434-84-7,79434-85-8,79434-86-9,79434-87-0,79434-88-1,104154-81-6,1406-70-8,54-22-8)

Guidance literature:

With toluene-4-sulfonic acid; In Ethylene carbonate; n-heptane; at 100 ℃; for 0.0833333h;

Reference yield:

(all-rac)-acetic acid 4-hydroxy-2,3,6-trimethyl-5-[3-(4,8,12-trimethyltridecyl)-but-3-enyl]phenyl ester (696597-97-4) → vitamin E acetate (58-95-7,7695-91-2,18920-61-1,52225-20-4,54165-54-7,66900-46-7,79200-45-6,79200-46-7,79200-47-8,79434-84-7,79434-85-8,79434-86-9,79434-87-0,79434-88-1,104154-81-6,1406-70-8,54-22-8)

Guidance literature:

toluene-4-sulfonic acid; In 1,2-propylene cyclic carbonate; n-heptane; at 120 ℃; for 1.5h;

upstream raw materials:

isophytol

4-acetoxy-2,3,5-trimethylphenol

Downstream raw materials:

vitamin E acetate

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