3-hydroxypropyl (4R,6S)-4-<(1R)-1-<(4-bromobenzoyl)oxy>ethyl>-6-methyloctanoate

Base Information

Chemical Name:3-hydroxypropyl (4R,6S)-4-<(1R)-1-<(4-bromobenzoyl)oxy>ethyl>-6-methyloctanoate
CAS No.:125228-66-2
Molecular Formula:C₂₁H₃₁BrO₅
Molecular Weight:443.378
Hs Code.:

Synonyms:3-hydroxypropyl (4R,6S)-4-<(1R)-1-<(4-bromobenzoyl)oxy>ethyl>-6-methyloctanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-hydroxypropyl (4R,6S)-4-<(1R)-1-<(4-bromobenzoyl)oxy>ethyl>-6-methyloctanoate

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Technology Process of 3-hydroxypropyl (4R,6S)-4-<(1R)-1-<(4-bromobenzoyl)oxy>ethyl>-6-methyloctanoate

There total 4 articles about 3-hydroxypropyl (4R,6S)-4-<(1R)-1-<(4-bromobenzoyl)oxy>ethyl>-6-methyloctanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 125228-65-1
2-<(3R,5S)-3-<(1R)-1-<(4-bromobenzoyl)oxy>ethyl>-5-methylheptyl>-1,3-dioxane

: 125228-66-2
3-hydroxypropyl (4R,6S)-4-<(1R)-1-<(4-bromobenzoyl)oxy>ethyl>-6-methyloctanoate

Guidance literature:: With sodium hypochlorite; acetic acid; In acetone; at 0 ℃; for 4h;
DOI:10.1021/jo00295a023

Reference yield:

: 586-76-5
4-Bromobenzoic acid

: 125228-66-2
3-hydroxypropyl (4R,6S)-4-<(1R)-1-<(4-bromobenzoyl)oxy>ethyl>-6-methyloctanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / 4-(dimethylamino)pyridine, 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / 22 h / 25 °C

2: 68 percent / glacial acetic acid, 5.25 percent aq. NaOCl / acetone / 4 h / 0 °C

With dmap; sodium hypochlorite; acetic acid; dicyclohexyl-carbodiimide; In dichloromethane; acetone;
DOI:10.1021/jo00295a023

Reference yield:

: 125228-64-0
2-<(3R,5S)-3-<(1R)-1-hydroxyethyl>-5-methylheptyl>-1,3-dioxane

: 125228-66-2
3-hydroxypropyl (4R,6S)-4-<(1R)-1-<(4-bromobenzoyl)oxy>ethyl>-6-methyloctanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / 4-(dimethylamino)pyridine, 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / 22 h / 25 °C

2: 68 percent / glacial acetic acid, 5.25 percent aq. NaOCl / acetone / 4 h / 0 °C

With dmap; sodium hypochlorite; acetic acid; dicyclohexyl-carbodiimide; In dichloromethane; acetone;
DOI:10.1021/jo00295a023