Benzyl 2-Acetamido-3-O-<(R)-1-carboxyethyl>-2-deoxy-α-D-glucopyranoside 1',4-Lactone

Base Information

Chemical Name:Benzyl 2-Acetamido-3-O-<(R)-1-carboxyethyl>-2-deoxy-α-D-glucopyranoside 1',4-Lactone
CAS No.:62959-83-5
Molecular Formula:C₁₈H₂₃NO₇
Molecular Weight:365.383
Hs Code.:

Synonyms:Benzyl 2-Acetamido-3-O-<(R)-1-carboxyethyl>-2-deoxy-α-D-glucopyranoside 1',4-Lactone

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Chemical Property of Benzyl 2-Acetamido-3-O-<(R)-1-carboxyethyl>-2-deoxy-α-D-glucopyranoside 1',4-Lactone

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Technology Process of Benzyl 2-Acetamido-3-O-<(R)-1-carboxyethyl>-2-deoxy-α-D-glucopyranoside 1',4-Lactone

There total 7 articles about Benzyl 2-Acetamido-3-O-<(R)-1-carboxyethyl>-2-deoxy-α-D-glucopyranoside 1',4-Lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 15892-26-9
benzyl 2-acetamido-3-O-<(R)-1-carboxyethyl>-2-deoxy-α-D-glucopyranoside

: 62959-83-5
Benzyl 2-Acetamido-3-O-<(R)-1-carboxyethyl>-2-deoxy-α-D-glucopyranoside 1',4-Lactone

Guidance literature:: With dicyclohexyl-carbodiimide; In 1,4-dioxane; Ambient temperature;
DOI:10.1016/0008-6215(84)85007-7

Reference yield:

: 39524-05-5
Benzyl 2-Acetamido-3-O-<(R)-1-carboxyethyl>-2-deoxy-α-D-glucopyranoside

: 62959-83-5
Benzyl 2-Acetamido-3-O-<(R)-1-carboxyethyl>-2-deoxy-α-D-glucopyranoside 1',4-Lactone

Guidance literature:: With toluene-4-sulfonic acid; In acetonitrile; for 3h; Yield given; Heating;
DOI:10.1021/jo00311a026

Reference yield:

: 10036-64-3
N-acetyl-D-glucosamine

: 62959-83-5
Benzyl 2-Acetamido-3-O-<(R)-1-carboxyethyl>-2-deoxy-α-D-glucopyranoside 1',4-Lactone

Guidance literature:: Multi-step reaction with 5 steps

1: HCl gas / 0.33 h / 95 °C

2: p-toluenesulfonic acid monohydrate / acetone / 2 h / Ambient temperature

3: 1) NaH / 1) THF, 2) 50 deg C, 18 h

4: acetic acid / ethanol; H₂O / 2 h / Heating

5: p-toluenesulfonic acid monohydrate / acetonitrile / 3 h / Heating

With hydrogenchloride; sodium hydride; toluene-4-sulfonic acid; acetic acid; In ethanol; water; acetone; acetonitrile;
DOI:10.1021/jo00311a026