3-(5-Oxo-1-phenyl-2-thioxo-imidazolidin-4-ylsulfanylthiocarbonylamino)-benzoic acid

Base Information

• Chemical Name: 3-(5-Oxo-1-phenyl-2-thioxo-imidazolidin-4-ylsulfanylthiocarbonylamino)-benzoic acid
• CAS No.: 165127-74-2
• Molecular Formula: C₁₇H₁₃N₃O₃S₃
• Molecular Weight: 403.507

Synonyms:3-(5-Oxo-1-phenyl-2-thioxo-imidazolidin-4-ylsulfanylthiocarbonylamino)-benzoic acid

Chemical Property of 3-(5-Oxo-1-phenyl-2-thioxo-imidazolidin-4-ylsulfanylthiocarbonylamino)-benzoic acid

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Technology Process of 3-(5-Oxo-1-phenyl-2-thioxo-imidazolidin-4-ylsulfanylthiocarbonylamino)-benzoic acid

There total 1 articles about 3-(5-Oxo-1-phenyl-2-thioxo-imidazolidin-4-ylsulfanylthiocarbonylamino)-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

3-Dithiocarboxyamino-benzoic acid + 5-bromo-3-phenyl-2-thiohydantoin → 3-(5-Oxo-1-phenyl-2-thioxo-imidazolidin-4-ylsulfanylthiocarbonylamino)-benzoic acid (165127-74-2)

Guidance literature:

With sodium acetate; In ethanol; for 2h; Heating;

DOI:10.1021/jf00057a038

Reference yield: 73.0%

3-(5-Oxo-1-phenyl-2-thioxo-imidazolidin-4-ylsulfanylthiocarbonylamino)-benzoic acid (165127-74-2) → 3-[4-Oxo-5-phenyl-6-thioxo-tetrahydro-imidazo[1,2-b][1,4,2]dithiazol-(2Z)-ylideneamino]-benzoic acid

Guidance literature:

With iodine; In ethanol; water; at 30 ℃;

DOI:10.1021/jf00057a038

Reference yield: 62.0%

3-(5-Oxo-1-phenyl-2-thioxo-imidazolidin-4-ylsulfanylthiocarbonylamino)-benzoic acid (165127-74-2) → 3-(7-Oxo-6-phenyl-2,5-dithioxo-tetrahydro-imidazo[5,1-b][1,3,4]thiadiazol-3-yl)-benzoyl chloride (165127-88-8)

Guidance literature:

With pyridine; thionyl chloride; for 8h; Heating;

DOI:10.1021/jf00057a038

Downstream raw materials:

3-(7-Oxo-6-phenyl-2,5-dithioxo-tetrahydro-imidazo[5,1-b][1,3,4]thiadiazol-3-yl)-benzoyl chloride

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