2-bromo-6-chloro-3-<oxy>-4-propylbenzenol

Base Information

Chemical Name:2-bromo-6-chloro-3-<oxy>-4-propylbenzenol
CAS No.:135145-43-6
Molecular Formula:C₁₅H₂₄BrClO₂Si
Molecular Weight:379.797
Hs Code.:

2-bromo-6-chloro-3-<<dimethyl(1,1-dimethylethyl)silyl>oxy>-4-propylbenzenol

Synonyms:2-bromo-6-chloro-3-<oxy>-4-propylbenzenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-bromo-6-chloro-3-<oxy>-4-propylbenzenol

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Technology Process of 2-bromo-6-chloro-3-<oxy>-4-propylbenzenol

There total 4 articles about 2-bromo-6-chloro-3-<oxy>-4-propylbenzenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2-Bromo-4-chloro-3-methoxy-6-propyl-phenoxy)-tert-butyl-dimethyl-silane

: 135145-43-6
2-bromo-6-chloro-3-<oxy>-4-propylbenzenol

Guidance literature:: With boron tribromide; In dichloromethane; at 0 ℃; for 1.5h; Yield given;
DOI:10.1021/jo00018a015

Reference yield:

: 85696-74-8
5-Methoxy-2-propyl-phenol

: 135145-43-6
2-bromo-6-chloro-3-<oxy>-4-propylbenzenol

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / SO₂Cl₂ / diethyl ether / 1.5 h

2: 92 percent / Br₂ / acetic acid / 0.75 h

3: 6.5 g / imidazole / dimethylformamide / 1.5 h

4: BBr₃ / CH₂Cl₂ / 1.5 h / 0 °C

With 1H-imidazole; sulfuryl dichloride; bromine; boron tribromide; In diethyl ether; dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jo00018a015

Reference yield:

: 135145-41-4
4-chloro-5-methoxy-2-propylbenzenol

: 135145-43-6
2-bromo-6-chloro-3-<oxy>-4-propylbenzenol

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / Br₂ / acetic acid / 0.75 h

2: 6.5 g / imidazole / dimethylformamide / 1.5 h

3: BBr₃ / CH₂Cl₂ / 1.5 h / 0 °C

With 1H-imidazole; bromine; boron tribromide; In dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jo00018a015