5-(4-amino-2,6-dichloro-phenoxy)-3-methyl-1H-indole-2-carboxylic acid isopropylamide

Base Information

Chemical Name:5-(4-amino-2,6-dichloro-phenoxy)-3-methyl-1H-indole-2-carboxylic acid isopropylamide
CAS No.:957828-52-3
Molecular Formula:C₁₉H₁₉Cl₂N₃O₂
Molecular Weight:392.285
Hs Code.:

Synonyms:5-(4-amino-2,6-dichloro-phenoxy)-3-methyl-1H-indole-2-carboxylic acid isopropylamide

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Chemical Property of 5-(4-amino-2,6-dichloro-phenoxy)-3-methyl-1H-indole-2-carboxylic acid isopropylamide

Chemical Property:

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Technology Process of 5-(4-amino-2,6-dichloro-phenoxy)-3-methyl-1H-indole-2-carboxylic acid isopropylamide

There total 4 articles about 5-(4-amino-2,6-dichloro-phenoxy)-3-methyl-1H-indole-2-carboxylic acid isopropylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 957828-51-2
5-(2,6-dichloro-4-nitro-phenoxy)-3-methyl-1H-indole-2-carboxylic acid isopropylamide

: 957828-52-3
5-(4-amino-2,6-dichloro-phenoxy)-3-methyl-1H-indole-2-carboxylic acid isopropylamide

Guidance literature:: With iron; acetic acid; In water; at 20 ℃; for 3h; Acidic aqueous solution;

Reference yield:

: 957828-50-1
5-hydroxy-3-methyl-1H-indole-2-carboxylic acid isopropylamide

: 957828-52-3
5-(4-amino-2,6-dichloro-phenoxy)-3-methyl-1H-indole-2-carboxylic acid isopropylamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / dimethyl sulfoxide / 17 h / 120 °C

2: iron; acetic acid / water / 3 h / 20 °C / Acidic aqueous solution

With iron; potassium carbonate; acetic acid; In water; dimethyl sulfoxide;

Reference yield:

: 16381-42-3
ethyl 5-methoxy-3-methyl-1H-indole-2-carboxylate

: 957828-52-3
5-(4-amino-2,6-dichloro-phenoxy)-3-methyl-1H-indole-2-carboxylic acid isopropylamide

Guidance literature:: Multi-step reaction with 5 steps

1: water / Alkaline aqueous solution

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 18 h / 0 - 20 °C

3: boron dimethyl-trifluoro sulphide / 0 °C

4: potassium carbonate / dimethyl sulfoxide / 17 h / 120 °C

5: iron; acetic acid / water / 3 h / 20 °C / Acidic aqueous solution

With boron dimethyl-trifluoro sulphide; water; iron; potassium carbonate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In water; dimethyl sulfoxide; N,N-dimethyl-formamide;