1,3-bis(3,5-bis[2-{2-(2-methoxyethoxy)ethoxy}ethoxy]benzyl)imidazolium bromide

Base Information

Chemical Name:1,3-bis(3,5-bis[2-{2-(2-methoxyethoxy)ethoxy}ethoxy]benzyl)imidazolium bromide
CAS No.:1609210-48-1
Molecular Formula:Br*C₄₅H₇₃N₂O₁₆
Molecular Weight:977.982
Hs Code.:

Synonyms:1,3-bis(3,5-bis[2-{2-(2-methoxyethoxy)ethoxy}ethoxy]benzyl)imidazolium bromide

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Chemical Property of 1,3-bis(3,5-bis[2-{2-(2-methoxyethoxy)ethoxy}ethoxy]benzyl)imidazolium bromide

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Technology Process of 1,3-bis(3,5-bis[2-{2-(2-methoxyethoxy)ethoxy}ethoxy]benzyl)imidazolium bromide

There total 1 articles about 1,3-bis(3,5-bis[2-{2-(2-methoxyethoxy)ethoxy}ethoxy]benzyl)imidazolium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 288-32-4
1H-imidazole

: 246140-08-9
3,5-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzylbromide

: 1609210-48-1
1,3-bis(3,5-bis[2-{2-(2-methoxyethoxy)ethoxy}ethoxy]benzyl)imidazolium bromide

Guidance literature:: With CsF-Celite; In N,N-dimethyl-formamide; at 90 ℃; for 24h;
DOI:10.1016/j.tetlet.2014.03.074

Reference yield: 91.0%

: dimethylsulfide gold(I) chloride

: 1609210-48-1
1,3-bis(3,5-bis[2-{2-(2-methoxyethoxy)ethoxy}ethoxy]benzyl)imidazolium bromide

: chloro{1,3-bis(3,5-bis[2-{2-(2-methoxyethoxy)ethoxy}ethoxy]benzyl)imidazol-2-ylidene}gold(I)

Guidance literature:: 1,3-bis(3,5-bis[2-{2-(2-methoxyethoxy)ethoxy}ethoxy]benzyl)imidazolium bromide; With silver(l) oxide; In 1,2-dichloro-ethane; at 70 ℃; for 5h;

dimethylsulfide gold(I) chloride; at 20 ℃; for 3h;
DOI:10.1016/j.tetlet.2014.03.074

Reference yield: 70.7%

: 29892-37-3
chloro(dimethylsulfide) gold(I)

: 1609210-48-1
1,3-bis(3,5-bis[2-{2-(2-methoxyethoxy)ethoxy}ethoxy]benzyl)imidazolium bromide

: chloro{1,3-bis(3,5-bis[2-{2-(2-methoxyethoxy)ethoxy}ethoxy]benzyl)imidazol-2-ylidene}gold(I)

Guidance literature:: 1,3-bis(3,5-bis[2-{2-(2-methoxyethoxy)ethoxy}ethoxy]benzyl)imidazolium bromide; With silver(l) oxide; In 1,2-dichloro-ethane; at 60 ℃; for 18h; Inert atmosphere;

chloro(dimethylsulfide) gold(I); In 1,2-dichloro-ethane; at 20 ℃; for 3h; Inert atmosphere;