[6,7-dimethoxy-4-(1H-tetrazol-5-yl)-isoquinolin-1-yl]-(3-ethoxy-phenyl)-methanone

Base Information

Chemical Name:[6,7-dimethoxy-4-(1H-tetrazol-5-yl)-isoquinolin-1-yl]-(3-ethoxy-phenyl)-methanone
CAS No.:798565-60-3
Molecular Formula:C₂₁H₁₉N₅O₄
Molecular Weight:405.413
Hs Code.:

Synonyms:[6,7-dimethoxy-4-(1H-tetrazol-5-yl)-isoquinolin-1-yl]-(3-ethoxy-phenyl)-methanone

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Chemical Property of [6,7-dimethoxy-4-(1H-tetrazol-5-yl)-isoquinolin-1-yl]-(3-ethoxy-phenyl)-methanone

Chemical Property:

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Technology Process of [6,7-dimethoxy-4-(1H-tetrazol-5-yl)-isoquinolin-1-yl]-(3-ethoxy-phenyl)-methanone

There total 11 articles about [6,7-dimethoxy-4-(1H-tetrazol-5-yl)-isoquinolin-1-yl]-(3-ethoxy-phenyl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 798565-62-5
1-(3-ethoxy-benzoyl)-6,7-dimethoxy-isoquinoline-4-carbonitrile

: 798565-60-3
[6,7-dimethoxy-4-(1H-tetrazol-5-yl)-isoquinolin-1-yl]-(3-ethoxy-phenyl)-methanone

Guidance literature:: With sodium azide; ammonium chloride; In DMF (N,N-dimethyl-formamide); at 120 ℃; for 24h;

Reference yield:

: 798565-62-5
1-(3-ethoxy-benzoyl)-6,7-dimethoxy-isoquinoline-4-carbonitrile

: 798565-60-3
C₂₁H₁₉N₅O₄

Guidance literature:: With sodium azide; ammonium chloride; In N,N-dimethyl-formamide; at 120 ℃;
DOI:10.1016/j.bmcl.2011.09.009

Reference yield:

: 798565-45-4
1-bromo-6,7-dimethoxyisoquinoline-4-carbonitrile

: 798565-60-3
C₂₁H₁₉N₅O₄

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride; 1,3-dimethylimidazolim iodide / N,N-dimethyl-formamide

2: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 120 °C

With sodium azide; sodium hydride; 1,3-dimethylimidazolim iodide; ammonium chloride; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.009