4-chloro-N-(prop-2-en-1-yl)-N-(2,2,2-trichloroethyl)benzenesulfonamide

Base Information

Chemical Name:4-chloro-N-(prop-2-en-1-yl)-N-(2,2,2-trichloroethyl)benzenesulfonamide
CAS No.:1430086-42-2
Molecular Formula:C₁₁H₁₁Cl₄NO₂S
Molecular Weight:363.092
Hs Code.:

Synonyms:4-chloro-N-(prop-2-en-1-yl)-N-(2,2,2-trichloroethyl)benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chloro-N-(prop-2-en-1-yl)-N-(2,2,2-trichloroethyl)benzenesulfonamide

Chemical Property:

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Technology Process of 4-chloro-N-(prop-2-en-1-yl)-N-(2,2,2-trichloroethyl)benzenesulfonamide

There total 3 articles about 4-chloro-N-(prop-2-en-1-yl)-N-(2,2,2-trichloroethyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 40888-37-7
4-chloro-N-(2,2,2-trichloroethyl)benzenesulfonamide

: 106-95-6
allyl bromide

: 1430086-42-2
4-chloro-N-(prop-2-en-1-yl)-N-(2,2,2-trichloroethyl)benzenesulfonamide

Guidance literature:: With potassium carbonate; In acetonitrile; at 60 ℃; for 6h;
DOI:10.1134/S1070428017060021

Reference yield:

: 40888-36-6
C₈H₆Cl₅NO₂S

: 1430086-42-2
4-chloro-N-(prop-2-en-1-yl)-N-(2,2,2-trichloroethyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogensulfite / chlorobenzene; water / 1 h / 20 °C / Inert atmosphere

2: potassium carbonate / acetonitrile / 6 h / 60 °C

With potassium carbonate; sodium hydrogensulfite; In water; chlorobenzene; acetonitrile;
DOI:10.1134/S1070428017060021

Reference yield:

: 17260-65-0
N,N-dichloro-4-chlorobenzenesulfonamide

: 1430086-42-2
4-chloro-N-(prop-2-en-1-yl)-N-(2,2,2-trichloroethyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: chlorobenzene / 4 h / 100 °C / Inert atmosphere

2: sodium hydrogensulfite / chlorobenzene; water / 1 h / 20 °C / Inert atmosphere

3: potassium carbonate / acetonitrile / 6 h / 60 °C

With potassium carbonate; sodium hydrogensulfite; In water; chlorobenzene; acetonitrile;
DOI:10.1134/S1070428017060021