[2'-(hydroxy-diphenyl-methyl)-6,6'-dimethyl-biphenyl-2-yl]-diphenyl-methanol

Base Information

Chemical Name:[2'-(hydroxy-diphenyl-methyl)-6,6'-dimethyl-biphenyl-2-yl]-diphenyl-methanol
CAS No.:461642-18-2
Molecular Formula:C₄₀H₃₄O₂
Molecular Weight:546.709
Hs Code.:

Synonyms:[2'-(hydroxy-diphenyl-methyl)-6,6'-dimethyl-biphenyl-2-yl]-diphenyl-methanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [2'-(hydroxy-diphenyl-methyl)-6,6'-dimethyl-biphenyl-2-yl]-diphenyl-methanol

Chemical Property:

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Technology Process of [2'-(hydroxy-diphenyl-methyl)-6,6'-dimethyl-biphenyl-2-yl]-diphenyl-methanol

There total 1 articles about [2'-(hydroxy-diphenyl-methyl)-6,6'-dimethyl-biphenyl-2-yl]-diphenyl-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 93878-26-3,83527-40-6,83527-41-7
dimethyl 6,6'-dimethylbiphenyl-2-2'-dicarboxylate

: 461642-18-2
[2'-(hydroxy-diphenyl-methyl)-6,6'-dimethyl-biphenyl-2-yl]-diphenyl-methanol

Guidance literature:: bromobenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

dimethyl 6,6'-dimethylbiphenyl-2-2'-dicarboxylate; In tetrahydrofuran; hexane; at -78 ℃; for 1h;
DOI:10.1021/jo060662s

Reference yield:

: 461642-18-2
[2'-(hydroxy-diphenyl-methyl)-6,6'-dimethyl-biphenyl-2-yl]-diphenyl-methanol

: 716337-48-3
(P,M)-1,11-dimethyl-5,5,7,7-tetraphenyl-5,7-dihydrodibenz[c,e]oxepine

Guidance literature:: With o-toluenesulfonic acid; In toluene; for 12h; Heating;
DOI:10.1107/S010827010400294X

Reference yield:

: 461642-18-2
[2'-(hydroxy-diphenyl-methyl)-6,6'-dimethyl-biphenyl-2-yl]-diphenyl-methanol

: 6,6'-dimethyl-1,1'-biphenyl-2,2'-diylbis(diphenylmethylium) diperchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / CH₂Cl₂ / 10 h / 20 °C

2: 97 percent / Me₃SiClO₄ / CH₂Cl₂; toluene / 24 h / 20 °C

With trimethylsilyl perchlorate; trifluoroacetic acid; In dichloromethane; toluene;
DOI:10.1021/jo060662s