4-(2-((2-((tert-butyldimethylsilyl)oxy)ethyl)(phenyl)amino)-2-oxoethyl)-N-hydroxybenzamide

Base Information

Chemical Name:4-(2-((2-((tert-butyldimethylsilyl)oxy)ethyl)(phenyl)amino)-2-oxoethyl)-N-hydroxybenzamide
CAS No.:1429653-16-6
Molecular Formula:C₂₃H₃₂N₂O₄Si
Molecular Weight:428.604
Hs Code.:

Synonyms:4-(2-((2-((tert-butyldimethylsilyl)oxy)ethyl)(phenyl)amino)-2-oxoethyl)-N-hydroxybenzamide

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Chemical Property of 4-(2-((2-((tert-butyldimethylsilyl)oxy)ethyl)(phenyl)amino)-2-oxoethyl)-N-hydroxybenzamide

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Technology Process of 4-(2-((2-((tert-butyldimethylsilyl)oxy)ethyl)(phenyl)amino)-2-oxoethyl)-N-hydroxybenzamide

There total 6 articles about 4-(2-((2-((tert-butyldimethylsilyl)oxy)ethyl)(phenyl)amino)-2-oxoethyl)-N-hydroxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1429653-12-2
methyl 4-(2-((2-((tert-butyldimethylsilyl)oxy)ethyl)(phenyl)amino)-2-oxoethyl)benzoate

: 1429653-16-6
4-(2-((2-((tert-butyldimethylsilyl)oxy)ethyl)(phenyl)amino)-2-oxoethyl)-N-hydroxybenzamide

Guidance literature:: With potassium cyanide; hydroxylamine; In tetrahydrofuran; methanol; water; at 20 ℃; for 16h; Inert atmosphere;

Reference yield:

: 22744-12-3
[4-(methoxycarbonyl)phenyl]acetic acid

: 1429653-16-6
4-(2-((2-((tert-butyldimethylsilyl)oxy)ethyl)(phenyl)amino)-2-oxoethyl)-N-hydroxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere

2: hydroxylamine; potassium cyanide / water; tetrahydrofuran; methanol / 16 h / 20 °C / Inert atmosphere

With potassium cyanide; hydroxylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; dichloromethane; water;

Reference yield:

: 73401-74-8
4-hydroxymethylphenylacetic acid

: 1429653-16-6
4-(2-((2-((tert-butyldimethylsilyl)oxy)ethyl)(phenyl)amino)-2-oxoethyl)-N-hydroxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid; calcium hypochlorite / acetonitrile / 48 h / 20 °C / Darkness; Inert atmosphere

1.2: pH Ca_.2

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere

3.1: hydroxylamine; potassium cyanide / water; tetrahydrofuran; methanol / 16 h / 20 °C / Inert atmosphere

With potassium cyanide; calcium hypochlorite; hydroxylamine; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;