tert-butyl azidoacetate

Base Information

• Chemical Name: tert-butyl azidoacetate
• CAS No.: 6367-36-8
• Molecular Formula: C6H11 N3 O2
• Molecular Weight: 157.172
• Mol file: 6367-36-8.mol

Synonyms:Aceticacid, azido-, 1,1-dimethylethyl ester (9CI); Acetic acid, azido-, tert-butylester (6CI,7CI,8CI); tert-Butyl azidoacetate

Chemical Property of tert-butyl azidoacetate

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tert-butyl azidoacetate

There total 3 articles about tert-butyl azidoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

bromoacetic acid tert-butyl ester (5292-43-3) → tert-butyl 2-azidoacetate (6367-36-8)

Guidance literature:

With Caswell No_. 744A; In dimethyl sulfoxide; at 20 ℃;

DOI:10.1016/j.bmc.2009.12.057

Reference yield:

tert-Butyl chloroacetate (107-59-5) → tert-butyl 2-azidoacetate (6367-36-8)

Guidance literature:

With sodium azide;

Reference yield:

→ tert-butyl 2-azidoacetate (6367-36-8)

Guidance literature:

With sodium azide;

DOI:10.1248/bpb.18.1805

upstream raw materials:

tert-Butyl chloroacetate

bromoacetic acid tert-butyl ester

Downstream raw materials:

Glycine tert-butyl ester

N-(tert-butoxycarbonyl)glycine tert-butyl ester