5,15-bis(4''-carboxymethyleneoxyphenyl)-10,20-bis(1',1',3',3'-tetramethyl-isoindolin-2'-yloxyl-5'-yl)-porphyrin

Base Information

• Chemical Name: 5,15-bis(4''-carboxymethyleneoxyphenyl)-10,20-bis(1',1',3',3'-tetramethyl-isoindolin-2'-yloxyl-5'-yl)-porphyrin
• CAS No.: 1370037-35-6
• Molecular Formula: C₆₀H₅₄N₆O₈
• Molecular Weight: 987.124

Synonyms:5,15-bis(4''-carboxymethyleneoxyphenyl)-10,20-bis(1',1',3',3'-tetramethyl-isoindolin-2'-yloxyl-5'-yl)-porphyrin

Chemical Property of 5,15-bis(4''-carboxymethyleneoxyphenyl)-10,20-bis(1',1',3',3'-tetramethyl-isoindolin-2'-yloxyl-5'-yl)-porphyrin

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Technology Process of 5,15-bis(4''-carboxymethyleneoxyphenyl)-10,20-bis(1',1',3',3'-tetramethyl-isoindolin-2'-yloxyl-5'-yl)-porphyrin

There total 3 articles about 5,15-bis(4''-carboxymethyleneoxyphenyl)-10,20-bis(1',1',3',3'-tetramethyl-isoindolin-2'-yloxyl-5'-yl)-porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

5,15-bis(4''-carboethoxymethylene-oxy-phenyl)-10,20-bis(1',1',3',3'-tetramethyl-isoindolin-2'-yloxyl-5'-yl)porphyrin (1370037-30-1) → 5,15-bis(4''-carboxymethyleneoxyphenyl)-10,20-bis(1',1',3',3'-tetramethyl-isoindolin-2'-yloxyl-5'-yl)-porphyrin (1370037-35-6)

Guidance literature:

With sodium hydroxide; In methanol; at 20 - 50 ℃; for 7h; pH=10; Inert atmosphere;

DOI:10.1142/S1088424611003203

Reference yield:

5-(4′-carboethoxymethyleneoxyphenyl)dipyrromethane (847375-27-3) → 5,15-bis(4''-carboxymethyleneoxyphenyl)-10,20-bis(1',1',3',3'-tetramethyl-isoindolin-2'-yloxyl-5'-yl)-porphyrin (1370037-35-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 1 h / 20 °C / Inert atmosphere; Darkness

1.2: 1 h / Inert atmosphere

2.1: sodium hydroxide / methanol / 7 h / 20 - 50 °C / pH 10 / Inert atmosphere

With boron trifluoride diethyl etherate; sodium hydroxide; In methanol; dichloromethane;

DOI:10.1142/S1088424611003203

Reference yield:

5-formyl-1,1,3,3-tetramethylisoindolin-2-yloxyl (276885-27-9) → 5,15-bis(4''-carboxymethyleneoxyphenyl)-10,20-bis(1',1',3',3'-tetramethyl-isoindolin-2'-yloxyl-5'-yl)-porphyrin (1370037-35-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 1 h / 20 °C / Inert atmosphere; Darkness

1.2: 1 h / Inert atmosphere

2.1: sodium hydroxide / methanol / 7 h / 20 - 50 °C / pH 10 / Inert atmosphere

With boron trifluoride diethyl etherate; sodium hydroxide; In methanol; dichloromethane;

DOI:10.1142/S1088424611003203

upstream raw materials:

5-(4′-carboethoxymethyleneoxyphenyl)dipyrromethane

5,15-bis(4''-carboethoxymethylene-oxy-phenyl)-10,20-bis(1',1',3',3'-tetramethyl-isoindolin-2'-yloxyl-5'-yl)porphyrin

5-formyl-1,1,3,3-tetramethylisoindolin-2-yloxyl

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