5,6-dideoxy-1,2-O-isopropylidene-3-O-(p-methoxyphenyl)methyl-6-C-(n-octyl)-α-D-xylo-hex-5-eno-furanose

Base Information

Chemical Name:5,6-dideoxy-1,2-O-isopropylidene-3-O-(p-methoxyphenyl)methyl-6-C-(n-octyl)-α-D-xylo-hex-5-eno-furanose
CAS No.:224297-56-7
Molecular Formula:C₂₅H₃₈O₅
Molecular Weight:418.574
Hs Code.:

Synonyms:5,6-dideoxy-1,2-O-isopropylidene-3-O-(p-methoxyphenyl)methyl-6-C-(n-octyl)-α-D-xylo-hex-5-eno-furanose

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Chemical Property of 5,6-dideoxy-1,2-O-isopropylidene-3-O-(p-methoxyphenyl)methyl-6-C-(n-octyl)-α-D-xylo-hex-5-eno-furanose

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Technology Process of 5,6-dideoxy-1,2-O-isopropylidene-3-O-(p-methoxyphenyl)methyl-6-C-(n-octyl)-α-D-xylo-hex-5-eno-furanose

There total 1 articles about 5,6-dideoxy-1,2-O-isopropylidene-3-O-(p-methoxyphenyl)methyl-6-C-(n-octyl)-α-D-xylo-hex-5-eno-furanose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82529-87-1
(3aR,5S,6S,6aR)-6-(4-methoxybenzyloxy)-tetrahydro-2,2-dimethylfuro[2,3-d][1,3]dioxole-5-carbaldehyde

: 60902-45-6
nonyltriphenylphosphonium bromide

: 224297-56-7
5,6-dideoxy-1,2-O-isopropylidene-3-O-(p-methoxyphenyl)methyl-6-C-(n-octyl)-α-D-xylo-hex-5-eno-furanose

Guidance literature:: With n-butyllithium; Yield given; Multistep reaction; 1.) THF, hexane, RT, 30 min, 2.) THF, hexane, 1 h;
DOI:10.1016/S0957-4166(99)00057-9

Reference yield: 93.0%

: 224297-56-7
5,6-dideoxy-1,2-O-isopropylidene-3-O-(p-methoxyphenyl)methyl-6-C-(n-octyl)-α-D-xylo-hex-5-eno-furanose

: 224297-53-4
5-deoxy-1,2-O-isopropylidene-3-O-(p-methoxyphenyl)methyl-5-C-(n-nonyl)-α-D-xylofuranose

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 12h; Ambient temperature;
DOI:10.1016/S0957-4166(99)00057-9

Reference yield:

: 224297-56-7
5,6-dideoxy-1,2-O-isopropylidene-3-O-(p-methoxyphenyl)methyl-6-C-(n-octyl)-α-D-xylo-hex-5-eno-furanose

: methyl 5-deoxy-3-O-(p-methoxyphenyl)methyl-5-C-(n-nonyl)-β-D-xylofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / H₂ / 5 percent Pd/C / ethanol / 12 h / Ambient temperature

2: 34 percent / Amberlite IR 120 H⁺ / 6 h / 60 °C

With Amberlite IR 120 H⁺; hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1016/S0957-4166(99)00057-9