3-(4-Fluoro-phenyl)-3-(2,2,2-trifluoro-acetylamino)-propionyl chloride

Base Information

Chemical Name:3-(4-Fluoro-phenyl)-3-(2,2,2-trifluoro-acetylamino)-propionyl chloride
CAS No.:117291-34-6
Molecular Formula:C₁₁H₈ClF₄NO₂
Molecular Weight:297.637
Hs Code.:

Synonyms:3-(4-Fluoro-phenyl)-3-(2,2,2-trifluoro-acetylamino)-propionyl chloride

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Chemical Property of 3-(4-Fluoro-phenyl)-3-(2,2,2-trifluoro-acetylamino)-propionyl chloride

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Technology Process of 3-(4-Fluoro-phenyl)-3-(2,2,2-trifluoro-acetylamino)-propionyl chloride

There total 3 articles about 3-(4-Fluoro-phenyl)-3-(2,2,2-trifluoro-acetylamino)-propionyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 117291-16-4
N-Trifluoroacetyl-p-fluoro-DL-phenylalanin

: 117291-34-6
3-(4-Fluoro-phenyl)-3-(2,2,2-trifluoro-acetylamino)-propionyl chloride

Guidance literature:: With thionyl chloride; for 0.5h; Heating;
DOI:10.1016/0223-5234(92)90029-Z

Reference yield:

: 459-57-4
4-fluorobenzaldehyde

: 117291-34-6
3-(4-Fluoro-phenyl)-3-(2,2,2-trifluoro-acetylamino)-propionyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium acetate / ethanol / 6 h / Heating

2: trifluoroacetic acid / 0.5 h / Heating

3: thionyl chloride / benzene / 0.5 h / Heating

With ammonium acetate; thionyl chloride; trifluoroacetic acid; In ethanol; benzene;

Reference yield:

: 325-89-3
3-amino-3-(4-fluorophenyl)propanoic acid

: 117291-34-6
3-(4-Fluoro-phenyl)-3-(2,2,2-trifluoro-acetylamino)-propionyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / 0.5 h / Heating

2: thionyl chloride / benzene / 0.5 h / Heating

With thionyl chloride; trifluoroacetic acid; In benzene;