C₃₃H₄₄O₉

Base Information

Chemical Name:C₃₃H₄₄O₉
CAS No.:1352816-12-6
Molecular Formula:C₃₃H₄₄O₉
Molecular Weight:584.707
Hs Code.:

C<sub>33</sub>H<sub>44</sub>O<sub>9</sub>

Synonyms:C₃₃H₄₄O₉

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₄₄O₉

Chemical Property:

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Technology Process of C₃₃H₄₄O₉

There total 10 articles about C₃₃H₄₄O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1352816-11-5
C₃₆H₄₈O₉

: 1352816-12-6
C₃₃H₄₄O₉

Guidance literature:: With cerium(III) chloride heptahydrate; oxalic acid; In acetonitrile; at 20 ℃; for 2h;
DOI:10.1002/anie.201104681

Reference yield:

: C₃₈H₅₆O₁₀Si

: 1352816-12-6
C₃₃H₄₄O₉

: 1352816-13-7
C₃₅H₄₈O₁₀

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1002/anie.201104681

Reference yield:

: 1352816-07-9
C₅₀H₆₄O₈Si

: 1352816-12-6
C₃₃H₄₄O₉

Guidance literature:: Multi-step reaction with 7 steps

1.1: o-xylene / 20 h / 165 °C / Inert atmosphere

2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

2.2: NaBO₃*4H₂O / 3 h / 20 °C

3.1: pyridine; dmap / dichloromethane / 1 h / 0 - 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 20 °C

5.1: pyridine; tributylphosphine / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

6.1: dihydrogen peroxide / dichloromethane; water / 29 h / 20 °C / pH 7 / aq. phosphate buffer

7.1: cerium(III) chloride heptahydrate; oxalic acid / acetonitrile / 2 h / 20 °C

With pyridine; dmap; tributylphosphine; cerium(III) chloride heptahydrate; tetrabutyl ammonium fluoride; dihydrogen peroxide; oxalic acid; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; o-xylene; water; acetonitrile; 2.1: Hydroboration reaction;
DOI:10.1002/anie.201104681