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tert-butyl 2-{[(4-aminophenyl)methyl](2-{4,7-bis[2-(tert-butoxy)-2-oxoethyl]-1,4,7-triazonan-1-yl}ethyl)amino}acetate

Base Information Edit
  • Chemical Name:tert-butyl 2-{[(4-aminophenyl)methyl](2-{4,7-bis[2-(tert-butoxy)-2-oxoethyl]-1,4,7-triazonan-1-yl}ethyl)amino}acetate
  • CAS No.:1258946-38-1
  • Molecular Formula:C33H57N5O6
  • Molecular Weight:619.845
  • Hs Code.:
  • Mol file:1258946-38-1.mol
tert-butyl 2-{[(4-aminophenyl)methyl](2-{4,7-bis[2-(tert-butoxy)-2-oxoethyl]-1,4,7-triazonan-1-yl}ethyl)amino}acetate

Synonyms:tert-butyl 2-{[(4-aminophenyl)methyl](2-{4,7-bis[2-(tert-butoxy)-2-oxoethyl]-1,4,7-triazonan-1-yl}ethyl)amino}acetate

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Chemical Property of tert-butyl 2-{[(4-aminophenyl)methyl](2-{4,7-bis[2-(tert-butoxy)-2-oxoethyl]-1,4,7-triazonan-1-yl}ethyl)amino}acetate Edit
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Technology Process of tert-butyl 2-{[(4-aminophenyl)methyl](2-{4,7-bis[2-(tert-butoxy)-2-oxoethyl]-1,4,7-triazonan-1-yl}ethyl)amino}acetate

There total 7 articles about tert-butyl 2-{[(4-aminophenyl)methyl](2-{4,7-bis[2-(tert-butoxy)-2-oxoethyl]-1,4,7-triazonan-1-yl}ethyl)amino}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 3 steps
1.1: oxalyl dichloride / dichloromethane; dimethyl sulfoxide / 2.17 h / -60 °C
1.2: 0.5 h / -60 °C
2.1: sodium tris(acetoxy)borohydride / dichloromethane / 18 h / 0 - 20 °C
3.1: hydrogen; palladium 10% on activated carbon / ethanol / 14 h / 20 °C / 1034.32 Torr / Inert atmosphere
With oxalyl dichloride; palladium 10% on activated carbon; hydrogen; sodium tris(acetoxy)borohydride; In ethanol; dichloromethane; dimethyl sulfoxide; 1.1: |Swern Oxidation;
DOI:10.1016/j.bmcl.2015.01.008
Guidance literature:
Multi-step reaction with 2 steps
1: sodium tris(acetoxy)borohydride / dichloromethane / 18 h / 0 - 20 °C
2: hydrogen; palladium 10% on activated carbon / ethanol / 14 h / 20 °C / 1034.32 Torr / Inert atmosphere
With palladium 10% on activated carbon; hydrogen; sodium tris(acetoxy)borohydride; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2015.01.008
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