benzyl (1R,2S)-2-(ethoxycarbonyl)-1-(2-cyanophenyl)-2-hydroxyethylcarbamate

Base Information

Chemical Name:benzyl (1R,2S)-2-(ethoxycarbonyl)-1-(2-cyanophenyl)-2-hydroxyethylcarbamate
CAS No.:1373919-74-4
Molecular Formula:C₂₀H₂₀N₂O₅
Molecular Weight:368.389
Hs Code.:

Synonyms:benzyl (1R,2S)-2-(ethoxycarbonyl)-1-(2-cyanophenyl)-2-hydroxyethylcarbamate

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Chemical Property of benzyl (1R,2S)-2-(ethoxycarbonyl)-1-(2-cyanophenyl)-2-hydroxyethylcarbamate

Chemical Property:

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Technology Process of benzyl (1R,2S)-2-(ethoxycarbonyl)-1-(2-cyanophenyl)-2-hydroxyethylcarbamate

There total 3 articles about benzyl (1R,2S)-2-(ethoxycarbonyl)-1-(2-cyanophenyl)-2-hydroxyethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 621-84-1
O-benzyl carbamate

: 50620-99-0
alpha-cyanocinnamic acid ethyl ester

: 1373919-74-4
benzyl (1R,2S)-2-(ethoxycarbonyl)-1-(2-cyanophenyl)-2-hydroxyethylcarbamate

: 1438105-51-1
C₁₂H₁₃NO₄

Guidance literature:: O-benzyl carbamate; With sodium hydroxide; In propan-1-ol; water; for 0.0333333h;

With tert-butylhypochlorite; In propan-1-ol; water;

alpha-cyanocinnamic acid ethyl ester; With potassium osmate; 1,4-bis(9-O-dihydroquinidine)phthalazine; In propan-1-ol; water;

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 1373919-74-4
benzyl (1R,2S)-2-(ethoxycarbonyl)-1-(2-cyanophenyl)-2-hydroxyethylcarbamate

: 1438105-51-1
C₁₂H₁₃NO₄

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 4 h / Reflux; Inert atmosphere

2: N,N-dimethyl-formamide / 18 h / Reflux; Inert atmosphere

3: sodium hydroxide / water; propan-1-ol / 0.03 h

With sodium hydroxide; In propan-1-ol; water; N,N-dimethyl-formamide; benzene;

Reference yield:

: 91047-77-7
ethyl (2E)-3-(2-bromophenyl)prop-2-enoate

: 1373919-74-4
benzyl (1R,2S)-2-(ethoxycarbonyl)-1-(2-cyanophenyl)-2-hydroxyethylcarbamate

: 1438105-51-1
C₁₂H₁₃NO₄

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 18 h / Reflux; Inert atmosphere

2: sodium hydroxide / water; propan-1-ol / 0.03 h

With sodium hydroxide; In propan-1-ol; water; N,N-dimethyl-formamide;