C₂₁H₂₆NO₂I

Base Information

Chemical Name:C₂₁H₂₆NO₂I
CAS No.:949146-00-3
Molecular Formula:C₂₁H₂₆INO₂
Molecular Weight:451.347
Hs Code.:

C<sub>21</sub>H<sub>26</sub>NO<sub>2</sub>I

Synonyms:C₂₁H₂₆NO₂I

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₂₆NO₂I

Chemical Property:

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Technology Process of C₂₁H₂₆NO₂I

There total 7 articles about C₂₁H₂₆NO₂I which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 949145-97-5
C₂₁H₂₇NO₃

: 949146-00-3
C₂₁H₂₆NO₂I

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In benzene; at 20 ℃; for 1h;
DOI:10.1021/jo0708137

Reference yield:

: 615-43-0
2-iodophenylamine

: 949146-00-3
C₂₁H₂₆NO₂I

Guidance literature:: Multi-step reaction with 7 steps

1: 90 percent / CuI; triethylamine / PdCl₂ / acetonitrile / 4 h / 20 °C

2: 85 percent / H₂ / Pd/C / methanol / 48 h / 20 °C

3: 85 percent / NaHCO₃ / dioxane; H₂O / 12 h / 20 °C

4: 95 percent / imidazole / CH₂Cl₂ / 2 h / 20 °C

5: 90 percent / NaH / tetrahydrofuran / 12 h / Heating

6: 98 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h

7: I₂; PPh₃; imidazole / benzene / 1 h / 20 °C

With 1H-imidazole; copper(l) iodide; tetrabutyl ammonium fluoride; hydrogen; iodine; sodium hydride; sodium hydrogencarbonate; triethylamine; triphenylphosphine; palladium on activated charcoal; palladium dichloride; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetonitrile; benzene;
DOI:10.1021/jo0708137

Reference yield:

: 125812-44-4
2-(2-(hydroxymethyl)ethynyl)aniline

: 949146-00-3
C₂₁H₂₆NO₂I

Guidance literature:: Multi-step reaction with 6 steps

1: 85 percent / H₂ / Pd/C / methanol / 48 h / 20 °C

2: 85 percent / NaHCO₃ / dioxane; H₂O / 12 h / 20 °C

3: 95 percent / imidazole / CH₂Cl₂ / 2 h / 20 °C

4: 90 percent / NaH / tetrahydrofuran / 12 h / Heating

5: 98 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h

6: I₂; PPh₃; imidazole / benzene / 1 h / 20 °C

With 1H-imidazole; tetrabutyl ammonium fluoride; hydrogen; iodine; sodium hydride; sodium hydrogencarbonate; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; benzene;
DOI:10.1021/jo0708137