pentacarbonyl{μ-{(η2:η2-ethynyl)benzene}}triphenylphosphinedicobalt-(Co-Co)

Base Information

Chemical Name:pentacarbonyl{μ-{(η2:η2-ethynyl)benzene}}triphenylphosphinedicobalt-(Co-Co)
CAS No.:55926-07-3
Molecular Formula:C₃₁H₂₁Co₂O₅P
Molecular Weight:622.465
Hs Code.:

Synonyms:pentacarbonyl{μ-{(η2:η2-ethynyl)benzene}}triphenylphosphinedicobalt-(Co-Co)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pentacarbonyl{μ-{(η2:η2-ethynyl)benzene}}triphenylphosphinedicobalt-(Co-Co)

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Technology Process of pentacarbonyl{μ-{(η2:η2-ethynyl)benzene}}triphenylphosphinedicobalt-(Co-Co)

There total 4 articles about pentacarbonyl{μ-{(η2:η2-ethynyl)benzene}}triphenylphosphinedicobalt-(Co-Co) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 12154-91-5
(phenylacetylene)hexacarbonyldicobalt

: 603-35-0
triphenylphosphine

: 55926-07-3
pentacarbonyl{μ-{(η2:η2-ethynyl)benzene}}triphenylphosphinedicobalt-(Co-Co)

Guidance literature:: In toluene; N2-atmosphere; equimolar amts., 60-70°C, 4 h; evapn. (vac.), chromy. (Al2O3); elem. anal.;
DOI:10.1016/0022-328X(95)06107-X

Reference yield: 84.0%

: 36116-67-3
2-butyne-3-onehexacarbonyldicobalt

: 603-35-0
triphenylphosphine

: 55926-07-3
pentacarbonyl{μ-{(η2:η2-ethynyl)benzene}}triphenylphosphinedicobalt-(Co-Co)

Guidance literature:: In toluene; Irradiation (UV/VIS); N2-atmosphere; equimolar amts., 351.1-363.8 nm laser, room temp., 7 h; evapn. (vac.), chromy. (Al2O3);
DOI:10.1016/0022-328X(95)06107-X

Reference yield: 45.0%

: 12154-91-5
(phenylacetylene)hexacarbonyldicobalt

: 55926-07-3
pentacarbonyl{μ-{(η2:η2-ethynyl)benzene}}triphenylphosphinedicobalt-(Co-Co)

Guidance literature:: With triphenylphosphine; In hexane; (N2); reflux the mixt. for 2-4 h;; concg. the soln. after filtration; chromy. (alumina column, diethyl ether/light petroleum);;
DOI:10.1016/0022-328X(88)87050-5