Technology Process of C22H24F2N2O5S
There total 4 articles about C22H24F2N2O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic anhydride; sodium iodide;
In
acetone;
at 0 ℃;
for 0.633333h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium azide / dichloromethane; acetone / 2 h / 0 °C / Inert atmosphere
2: benzene / 40 h / Reflux
3: copper(I) oxide / dichloromethane; diethyl ether / 43 h / -20 - 20 °C / Inert atmosphere
4: water; aluminum oxide / chloroform / 72 h / 20 °C / Inert atmosphere
5: sodium iodide; trifluoroacetic anhydride / acetone / 0.63 h / 0 °C / Inert atmosphere
With
copper(I) oxide; aluminum oxide; sodium azide; water; trifluoroacetic anhydride; sodium iodide;
In
diethyl ether; dichloromethane; chloroform; acetone; benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: benzene / 40 h / Reflux
2: copper(I) oxide / dichloromethane; diethyl ether / 43 h / -20 - 20 °C / Inert atmosphere
3: water; aluminum oxide / chloroform / 72 h / 20 °C / Inert atmosphere
4: sodium iodide; trifluoroacetic anhydride / acetone / 0.63 h / 0 °C / Inert atmosphere
With
copper(I) oxide; aluminum oxide; water; trifluoroacetic anhydride; sodium iodide;
In
diethyl ether; dichloromethane; chloroform; acetone; benzene;