benzyl cobactin T

Base Information

Chemical Name:benzyl cobactin T
CAS No.:77629-24-4
Molecular Formula:C₁₇H₂₄N₂O₄
Molecular Weight:320.389
Hs Code.:

Synonyms:benzyl cobactin T

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Chemical Property of benzyl cobactin T

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Technology Process of benzyl cobactin T

There total 6 articles about benzyl cobactin T which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 625-72-9,26063-00-3,29435-48-1
(R)-3-hydroxybutyric acid

: 77611-42-8
L-α-amino-N-(benzyloxy)caprolactam

: 77629-24-4
benzyl cobactin T

Guidance literature:: With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In tetrahydrofuran; at 50 ℃; for 22h;
DOI:10.1021/ja00340a017

Reference yield: 62.0%

: 1007123-23-0
(S)-3-amino-1-(benzyloxy)azepan-2-one hydrobromide

: 625-72-9,26063-00-3,29435-48-1
(R)-3-hydroxybutyric acid

: 77629-24-4
benzyl cobactin T

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 22 ℃; for 25h; Inert atmosphere;
DOI:10.1039/c2ob26077h

Reference yield:

: 77611-39-3
L-N_α-Boc-α-amino-N-(benzyloxy)caprolactame

: 77629-24-4
benzyl cobactin T

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / CF₃COOH / 0.08 h / Ambient temperature

2: 79 percent / EEDQ / tetrahydrofuran / 22 h / 50 °C

With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1021/ja00340a017