C₅₀H₇₅NO₁₀Si₂

Base Information

Chemical Name:C₅₀H₇₅NO₁₀Si₂
CAS No.:1402588-80-0
Molecular Formula:C₅₀H₇₅NO₁₀Si₂
Molecular Weight:906.317
Hs Code.:

C<sub>50</sub>H<sub>75</sub>NO<sub>10</sub>Si<sub>2</sub>

Synonyms:C₅₀H₇₅NO₁₀Si₂

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Chemical Property of C₅₀H₇₅NO₁₀Si₂

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Technology Process of C₅₀H₇₅NO₁₀Si₂

There total 15 articles about C₅₀H₇₅NO₁₀Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1402588-79-7
C₅₀H₇₃NO₉Si₂

: 1402588-80-0
C₅₀H₇₅NO₁₀Si₂

Guidance literature:: In ethanol; water; for 1.33333h; Reflux;
DOI:10.1021/ja3057612

Reference yield:

: C₁₈H₃₅NO₃Si

: 1402588-80-0
C₅₀H₇₅NO₁₀Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: Dess-Martin periodane / 3 h / 0 °C / Inert atmosphere

2: phenylborondichloride; N-ethyl-N,N-diisopropylamine / dichloromethane; methanol / 3.5 h / -78 °C / Inert atmosphere

3: benzo[1,3,2]dioxaborole / tetrahydrofuran / 20 h / -78 - 0 °C / Inert atmosphere

4: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere

5: water; ethanol / 1.33 h / Reflux

With 2,6-dimethylpyridine; phenylborondichloride; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; benzo[1,3,2]dioxaborole; In tetrahydrofuran; methanol; ethanol; dichloromethane; water;
DOI:10.1021/ja3057612

Reference yield:

: 38064-90-3
2,4-dimethoxytoluene

: 1402588-80-0
C₅₀H₇₅NO₁₀Si₂

Guidance literature:: Multi-step reaction with 14 steps

1: 6 h / 0 °C / Inert atmosphere

2: Inert atmosphere

3: thionyl chloride / benzene / 2 h / Reflux

4: 0 - 20 °C / Inert atmosphere

5: sec.-butyllithium / cyclohexane / 1 h / -78 °C / Inert atmosphere

6: boron tribromide / dichloromethane / 5.5 h / -78 - 25 °C / Inert atmosphere

7: dichloromethane / 20 h / 20 °C / Inert atmosphere

8: potassium carbonate / N,N-dimethyl-formamide / 20 h / 80 °C / Inert atmosphere

9: 4-methylmorpholine N-oxide; osmium(VIII) oxide / tetrahydrofuran; tert-butyl alcohol; water / 12 h / Inert atmosphere

10: sodium periodate / methanol / 1 h / 20 °C / Inert atmosphere

11: phenylborondichloride; N-ethyl-N,N-diisopropylamine / dichloromethane; methanol / 3.5 h / -78 °C / Inert atmosphere

12: benzo[1,3,2]dioxaborole / tetrahydrofuran / 20 h / -78 - 0 °C / Inert atmosphere

13: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere

14: water; ethanol / 1.33 h / Reflux

With 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; thionyl chloride; phenylborondichloride; sec.-butyllithium; boron tribromide; potassium carbonate; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; benzo[1,3,2]dioxaborole; In tetrahydrofuran; methanol; ethanol; dichloromethane; cyclohexane; water; N,N-dimethyl-formamide; tert-butyl alcohol; benzene;
DOI:10.1021/ja3057612