4,4'-bis-(triphenylphoshine)gold(I)-μ-2,3,5,6,2',3',5',6'-octafluoro-1,1'-biphenyl

Base Information

Chemical Name:4,4'-bis-(triphenylphoshine)gold(I)-μ-2,3,5,6,2',3',5',6'-octafluoro-1,1'-biphenyl
CAS No.:90635-35-1
Molecular Formula:C₄₈H₃₀Au₂F₈P₂
Molecular Weight:1214.63
Hs Code.:

Synonyms:4,4'-bis-(triphenylphoshine)gold(I)-μ-2,3,5,6,2',3',5',6'-octafluoro-1,1'-biphenyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4'-bis-(triphenylphoshine)gold(I)-μ-2,3,5,6,2',3',5',6'-octafluoro-1,1'-biphenyl

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Technology Process of 4,4'-bis-(triphenylphoshine)gold(I)-μ-2,3,5,6,2',3',5',6'-octafluoro-1,1'-biphenyl

There total 2 articles about 4,4'-bis-(triphenylphoshine)gold(I)-μ-2,3,5,6,2',3',5',6'-octafluoro-1,1'-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 90635-27-1
[(μ-4,4'-C6F4C6F4)(Au(tetrahydrothiophene))2]

: 90635-35-1
4,4'-bis-(triphenylphoshine)gold(I)-μ-2,3,5,6,2',3',5',6'-octafluoro-1,1'-biphenyl

Guidance literature:: With PPh₃; In dichloromethane; to CH2Cl2 soln. of complex added ligand, stirred at room temp. for 10 h; concd., pptd. (hexane); elem. anal.;
DOI:10.1016/0022-328X(84)85015-9

Reference yield: 60.0%

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 10386-84-2
4,4'-dibromo-2,3,5,6,2',3',5',6'-octafluoro-1,1'-biphenyl

: 90635-35-1
4,4'-bis-(triphenylphoshine)gold(I)-μ-2,3,5,6,2',3',5',6'-octafluoro-1,1'-biphenyl

Guidance literature:: With BuLi; In diethyl ether; (Ar); Schlenk techniques; 4,4'-dibromo-2,3,5,6,2',3',5',6'-octafluoro-1,1'-biphenyl cooled to -75°C in Et2O; BuLi added; stirred for 10 min; Cl(Ph3P)Au added; stirred for 10 min; warmed to room temp. over 1 h; filtered; vac. evapn.; recrystd. from Et2O; elem. anal.;
DOI:10.1515/znb-2009-11-1227