benzyl 3-[(+/-)-cyano[1R-cis-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarbonyloxy]methyl]phenoxyacetate

Base Information

Chemical Name:benzyl 3-[(+/-)-cyano[1R-cis-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarbonyloxy]methyl]phenoxyacetate
CAS No.:474457-46-0
Molecular Formula:C₂₅H₂₃Br₂NO₅
Molecular Weight:577.269
Hs Code.:

Synonyms:benzyl 3-[(+/-)-cyano[1R-cis-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarbonyloxy]methyl]phenoxyacetate

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Chemical Property of benzyl 3-[(+/-)-cyano[1R-cis-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarbonyloxy]methyl]phenoxyacetate

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Technology Process of benzyl 3-[(+/-)-cyano[1R-cis-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarbonyloxy]methyl]phenoxyacetate

There total 2 articles about benzyl 3-[(+/-)-cyano[1R-cis-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarbonyloxy]methyl]phenoxyacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53179-78-5,59952-39-5,61914-48-5,63538-10-3,63597-73-9,63949-77-9,72691-16-8,72691-18-0,74560-76-2
2,2-dimethyl-3R-(2',2'-dibromovinyl)-cyclopropane-1R-carboxylic acid

: 474457-46-0
benzyl 3-[(+/-)-cyano[1R-cis-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarbonyloxy]methyl]phenoxyacetate

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂; DMF / CHCl₃ / 1 h / 60 - 65 °C

2: 90 percent / pyridine / CHCl₃ / 0.5 h / 20 °C

With pyridine; thionyl chloride; N,N-dimethyl-formamide; In chloroform;
DOI:10.1021/jf0207629

Reference yield:

: 208251-96-1
(3-formylphenoxy)acetic acid benzyl ester

: 474457-46-0
benzyl 3-[(+/-)-cyano[1R-cis-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarbonyloxy]methyl]phenoxyacetate

Guidance literature:: Multi-step reaction with 2 steps

1: ZnI₂ / CHCl₃ / 2.5 h / 20 °C

2: 90 percent / pyridine / CHCl₃ / 0.5 h / 20 °C

With pyridine; zinc(II) iodide; In chloroform;
DOI:10.1021/jf0207629