(4S,5S,6S)-7-Benzyloxymethoxy-5-methoxymethoxy-4,6-dimethyl-heptanoic acid ethyl ester

Base Information

Chemical Name:(4S,5S,6S)-7-Benzyloxymethoxy-5-methoxymethoxy-4,6-dimethyl-heptanoic acid ethyl ester
CAS No.:204202-36-8
Molecular Formula:C₂₁H₃₄O₆
Molecular Weight:382.497
Hs Code.:

Synonyms:(4S,5S,6S)-7-Benzyloxymethoxy-5-methoxymethoxy-4,6-dimethyl-heptanoic acid ethyl ester

Suppliers and Price of (4S,5S,6S)-7-Benzyloxymethoxy-5-methoxymethoxy-4,6-dimethyl-heptanoic acid ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (4S,5S,6S)-7-Benzyloxymethoxy-5-methoxymethoxy-4,6-dimethyl-heptanoic acid ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (4S,5S,6S)-7-Benzyloxymethoxy-5-methoxymethoxy-4,6-dimethyl-heptanoic acid ethyl ester

There total 8 articles about (4S,5S,6S)-7-Benzyloxymethoxy-5-methoxymethoxy-4,6-dimethyl-heptanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 204202-35-7
(E)-(4S,5S,6S)-7-Benzyloxymethoxy-5-methoxymethoxy-4,6-dimethyl-hept-2-enoic acid ethyl ester

: 204202-36-8
(4S,5S,6S)-7-Benzyloxymethoxy-5-methoxymethoxy-4,6-dimethyl-heptanoic acid ethyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 14h; under 760 Torr;
DOI:10.1016/S0957-4166(97)00596-X

Reference yield:

: 204202-33-5
(2S,3S,4S)-5-Benzyloxymethoxy-3-methoxymethoxy-2,4-dimethyl-pentan-1-ol

: 204202-36-8
(4S,5S,6S)-7-Benzyloxymethoxy-5-methoxymethoxy-4,6-dimethyl-heptanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) (COCl)2, DMSO, 2.) Et₃N / 1.) CH₂Cl₂, -78 deg C, 15 min, 2.) CH₂Cl₂, -78 deg C, 15 min

2: 1.) NaH / 1.) THF, 15 min, 2.) THF, 18 h

3: 79 percent / H₂ / 10percent Pd/C / ethyl acetate / 14 h / 760 Torr

With oxalyl dichloride; hydrogen; sodium hydride; dimethyl sulfoxide; triethylamine; palladium on activated charcoal; In ethyl acetate;
DOI:10.1016/S0957-4166(97)00596-X

Reference yield:

: 204202-34-6
(2R,3R,4S)-5-Benzyloxymethoxy-3-methoxymethoxy-2,4-dimethyl-pentanal

: 204202-36-8
(4S,5S,6S)-7-Benzyloxymethoxy-5-methoxymethoxy-4,6-dimethyl-heptanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) THF, 15 min, 2.) THF, 18 h

2: 79 percent / H₂ / 10percent Pd/C / ethyl acetate / 14 h / 760 Torr

With hydrogen; sodium hydride; palladium on activated charcoal; In ethyl acetate;
DOI:10.1016/S0957-4166(97)00596-X