C₄₄H₆₄O₁₁

Base Information

Chemical Name:C₄₄H₆₄O₁₁
CAS No.:1263362-19-1
Molecular Formula:C₄₄H₆₄O₁₁
Molecular Weight:768.986
Hs Code.:

C<sub>44</sub>H<sub>64</sub>O<sub>11</sub>

Synonyms:C₄₄H₆₄O₁₁

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Chemical Property of C₄₄H₆₄O₁₁

Chemical Property:

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Technology Process of C₄₄H₆₄O₁₁

There total 17 articles about C₄₄H₆₄O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1263362-18-0
C₂₃H₃₄O₈

: 252679-40-6
diethyl (4-((2E)-3,7-dimethyl-2,6-octadienyl)-3,5-bis(methoxymethoxy)benzyl)phoshonate

: 1263362-19-1
C₄₄H₆₄O₁₁

Guidance literature:: diethyl (4-((2E)-3,7-dimethyl-2,6-octadienyl)-3,5-bis(methoxymethoxy)benzyl)phoshonate; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexanes; for 0.0833333h; Inert atmosphere; Cooling with ice;

C₂₃H₃₄O₈; In tetrahydrofuran; hexanes; for 2h; Inert atmosphere; Cooling with ice;

With potassium hexamethylsilazane; In tetrahydrofuran; hexanes; toluene; for 2h; Inert atmosphere; Cooling with ice;
DOI:10.1021/jo1022102

Reference yield:

: 1263362-61-3
C₁₅H₁₅BrO₃

: 1263362-19-1
C₄₄H₆₄O₁₁

Guidance literature:: Multi-step reaction with 15 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C / Inert atmosphere

2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / hexanes; diethyl ether / 15 h / Inert atmosphere; Cooling

2.2: 0.25 h / Inert atmosphere; Cooling

2.3: 20 °C / Inert atmosphere; Cooling

3.1: boron trifluoride diethyl etherate / dichloromethane / 0.13 h / -78 °C / Inert atmosphere

3.2: 23 h / 20 °C / 760.05 Torr

4.1: manganese(IV) oxide / dichloromethane / 20 h / 20 °C / Inert atmosphere

5.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere

5.2: 20 h / 20 °C / Inert atmosphere

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere

7.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 26 h / 20 °C / Inert atmosphere

8.1: potassium hydroxide / ethanol / 0.42 h / 20 °C / Inert atmosphere

9.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / dichloromethane / 2 h / 20 °C / Inert atmosphere

10.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / 1,4-dioxane; tert-butyl alcohol / 17 h / 20 °C

11.1: sodium periodate; water / dichloromethane / 24 h / 20 °C

12.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.25 h / 20 °C / Inert atmosphere

13.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran; water / 0.25 h / 20 °C

14.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 5.33 h / 20 °C / Inert atmosphere

15.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexanes / 0.08 h / Inert atmosphere; Cooling with ice

15.2: 2 h / Inert atmosphere; Cooling with ice

15.3: 2 h / Inert atmosphere; Cooling with ice

With manganese(IV) oxide; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; n-butyllithium; tetrapropylammonium perruthennate; N,N,N,N,-tetramethylethylenediamine; cerium(III) chloride heptahydrate; boron trifluoride diethyl etherate; water; sodium hydride; 4-methylmorpholine N-oxide; diisopropylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; diethyl ether; ethanol; dichloromethane; water; mineral oil; tert-butyl alcohol;
DOI:10.1021/jo1022102

Reference yield:

: 1263362-04-4
C₂₆H₃₄O₄

: 1263362-19-1
C₄₄H₆₄O₁₁

Guidance literature:: Multi-step reaction with 13 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 0.13 h / -78 °C / Inert atmosphere

1.2: 23 h / 20 °C / 760.05 Torr

2.1: manganese(IV) oxide / dichloromethane / 20 h / 20 °C / Inert atmosphere

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere

3.2: 20 h / 20 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere

5.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 26 h / 20 °C / Inert atmosphere

6.1: potassium hydroxide / ethanol / 0.42 h / 20 °C / Inert atmosphere

7.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / dichloromethane / 2 h / 20 °C / Inert atmosphere

8.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / 1,4-dioxane; tert-butyl alcohol / 17 h / 20 °C

9.1: sodium periodate; water / dichloromethane / 24 h / 20 °C

10.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.25 h / 20 °C / Inert atmosphere

11.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran; water / 0.25 h / 20 °C

12.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 5.33 h / 20 °C / Inert atmosphere

13.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexanes / 0.08 h / Inert atmosphere; Cooling with ice

13.2: 2 h / Inert atmosphere; Cooling with ice

13.3: 2 h / Inert atmosphere; Cooling with ice

With manganese(IV) oxide; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; n-butyllithium; tetrapropylammonium perruthennate; cerium(III) chloride heptahydrate; boron trifluoride diethyl etherate; water; 4-methylmorpholine N-oxide; diisopropylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; ethanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/jo1022102