1,1-dimethyl-3-phenylpropyl N-(diphenoxyphosphoryl)diphenylphosphinimidate

Base Information

Chemical Name:1,1-dimethyl-3-phenylpropyl N-(diphenoxyphosphoryl)diphenylphosphinimidate
CAS No.:913542-28-6
Molecular Formula:C₃₅H₃₅NO₄P₂
Molecular Weight:595.615
Hs Code.:

Synonyms:1,1-dimethyl-3-phenylpropyl N-(diphenoxyphosphoryl)diphenylphosphinimidate

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Chemical Property of 1,1-dimethyl-3-phenylpropyl N-(diphenoxyphosphoryl)diphenylphosphinimidate

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Technology Process of 1,1-dimethyl-3-phenylpropyl N-(diphenoxyphosphoryl)diphenylphosphinimidate

There total 3 articles about 1,1-dimethyl-3-phenylpropyl N-(diphenoxyphosphoryl)diphenylphosphinimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 26386-88-9
diphenyl phosphoryl azide

: 820961-79-3
1,1-dimethyl-3-phenylpropyl diphenylphosphinite

: 913542-28-6
1,1-dimethyl-3-phenylpropyl N-(diphenoxyphosphoryl)diphenylphosphinimidate

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1246/bcsj.79.1255

Reference yield:

: 103-05-9
4-phenyl-2-methyl-2-butanol

: 913542-28-6
1,1-dimethyl-3-phenylpropyl N-(diphenoxyphosphoryl)diphenylphosphinimidate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / DMAP; Et₃N / tetrahydrofuran / 2 h / 20 °C

2: 96 percent / tetrahydrofuran / 1 h / 0 °C

With dmap; triethylamine; In tetrahydrofuran;
DOI:10.1246/bcsj.79.1255

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 913542-28-6
1,1-dimethyl-3-phenylpropyl N-(diphenoxyphosphoryl)diphenylphosphinimidate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / DMAP; Et₃N / tetrahydrofuran / 2 h / 20 °C

2: 96 percent / tetrahydrofuran / 1 h / 0 °C

With dmap; triethylamine; In tetrahydrofuran;
DOI:10.1246/bcsj.79.1255