(1S,3S)-3-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-1-methyl-5-hexenyl-4-(benzyloxy)-6-heptenoate

Base Information

Chemical Name:(1S,3S)-3-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-1-methyl-5-hexenyl-4-(benzyloxy)-6-heptenoate
CAS No.:1041993-94-5
Molecular Formula:C₃₇H₄₈O₄Si
Molecular Weight:584.871
Hs Code.:

Synonyms:(1S,3S)-3-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-1-methyl-5-hexenyl-4-(benzyloxy)-6-heptenoate

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Chemical Property of (1S,3S)-3-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-1-methyl-5-hexenyl-4-(benzyloxy)-6-heptenoate

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Technology Process of (1S,3S)-3-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-1-methyl-5-hexenyl-4-(benzyloxy)-6-heptenoate

There total 1 articles about (1S,3S)-3-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-1-methyl-5-hexenyl-4-(benzyloxy)-6-heptenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1041994-09-5
4-(benzyloxy)-6-heptenoic acid

: 1041993-90-1
(2S,4S)-4-{[1-(tert-butyl)-1,1-diphenylsilyl]oxy}-6-hepten-2-ol

: 1041993-94-5
(1S,3S)-3-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-1-methyl-5-hexenyl-4-(benzyloxy)-6-heptenoate

Guidance literature:: 4-(benzyloxy)-6-heptenoic acid; With 2,4,6-trichlorobenzoyl chloride; triethylamine; In tetrahydrofuran; at 20 ℃; for 2h;

(2S,4S)-4-{[1-(tert-butyl)-1,1-diphenylsilyl]oxy}-6-hepten-2-ol; With dmap; In toluene; for 6h; Further stages.;
DOI:10.1016/j.tetasy.2008.04.016

Reference yield: 72.0%

: 1041993-94-5
(1S,3S)-3-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-1-methyl-5-hexenyl-4-(benzyloxy)-6-heptenoate

: 1041993-98-9
(10S,12S)-5-[1-(benzyloxy)]-10-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-12-methyl-1-oxa-7-cyclododecen-2-one

Guidance literature:: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; for 12h; Heating;
DOI:10.1016/j.tetasy.2008.04.016