4a,8a-diaza-2,6-dioxa-3,4,7,8,9,9a-hexahydro-9,9a-(1'-phenyl-2',5'-dioxo-1',3',4'-triazoline-3',4'-diyl)-4,4,8,8-tetramethylanthracene-1,5,-dione

Base Information

Chemical Name:4a,8a-diaza-2,6-dioxa-3,4,7,8,9,9a-hexahydro-9,9a-(1'-phenyl-2',5'-dioxo-1',3',4'-triazoline-3',4'-diyl)-4,4,8,8-tetramethylanthracene-1,5,-dione
CAS No.:142068-61-9
Molecular Formula:C₂₂H₂₃N₅O₆
Molecular Weight:453.455
Hs Code.:

Synonyms:4a,8a-diaza-2,6-dioxa-3,4,7,8,9,9a-hexahydro-9,9a-(1'-phenyl-2',5'-dioxo-1',3',4'-triazoline-3',4'-diyl)-4,4,8,8-tetramethylanthracene-1,5,-dione

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Chemical Property of 4a,8a-diaza-2,6-dioxa-3,4,7,8,9,9a-hexahydro-9,9a-(1'-phenyl-2',5'-dioxo-1',3',4'-triazoline-3',4'-diyl)-4,4,8,8-tetramethylanthracene-1,5,-dione

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Technology Process of 4a,8a-diaza-2,6-dioxa-3,4,7,8,9,9a-hexahydro-9,9a-(1'-phenyl-2',5'-dioxo-1',3',4'-triazoline-3',4'-diyl)-4,4,8,8-tetramethylanthracene-1,5,-dione

There total 2 articles about 4a,8a-diaza-2,6-dioxa-3,4,7,8,9,9a-hexahydro-9,9a-(1'-phenyl-2',5'-dioxo-1',3',4'-triazoline-3',4'-diyl)-4,4,8,8-tetramethylanthracene-1,5,-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 4233-33-4
4-Phenyl-1,2,4-triazolidine-3,5-dione

: 135005-65-1
4a,8a-diaza-2,6-dioxa-3,4,7,8-tetrahydro-4,4,8,8-tetramethylanthracene-1,5-dione

: 142068-61-9
4a,8a-diaza-2,6-dioxa-3,4,7,8,9,9a-hexahydro-9,9a-(1'-phenyl-2',5'-dioxo-1',3',4'-triazoline-3',4'-diyl)-4,4,8,8-tetramethylanthracene-1,5,-dione

Guidance literature:: In dichloromethane; for 0.0166667h;
DOI:10.1021/ja00041a018

Reference yield:

: 135005-70-8
3-(chloromethyl)-5,6-dihydro-5,5-dimethyl-1,4-oxazin-2-one

: 142068-61-9
4a,8a-diaza-2,6-dioxa-3,4,7,8,9,9a-hexahydro-9,9a-(1'-phenyl-2',5'-dioxo-1',3',4'-triazoline-3',4'-diyl)-4,4,8,8-tetramethylanthracene-1,5,-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 22 percent / (i-Pr)2NEt / dimethylformamide / 24 h / 95 °C

2: 53 percent / CH₂Cl₂ / 0.02 h

With N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00041a018